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(E)-N'-苄叉基-2-甲氧基苯甲酰肼的晶体结构

Crystal structure of (E)-N'-benzyl-idene-2-meth-oxy-benzohydrazide.

作者信息

Taha Muhammad, Baharudin M Syukri, Zaki Hamizah Mohd, Yamin Bohari M, Naz Humera

机构信息

Atta-ur-Rahman Institute for Natural Product Discovery, Universiti Teknologi MARA (UiTM), Puncak Alam Campus, 42300 Bandar Puncak Alam, Selangor D.E., Malaysia ; Faculty of Applied Science, Universiti Teknologi MARA (UiTM), 40450 Shah Alam, Selangor D.E., Malaysia.

Atta-ur-Rahman Institute for Natural Product Discovery, Universiti Teknologi MARA (UiTM), Puncak Alam Campus, 42300 Bandar Puncak Alam, Selangor D.E., Malaysia.

出版信息

Acta Crystallogr Sect E Struct Rep Online. 2014 Aug 30;70(Pt 9):o1071-2. doi: 10.1107/S1600536814019011. eCollection 2014 Sep 1.

Abstract

In the title benzoyl-hydrazide derivative, C15H14N2O2, the dihedral angle between the planes of the two phenyl rings is 12.56 (9)°. The azomethine double bond adopts an E configuration stabilized by an N-H⋯O hydrogen bond. In the crystal, the components are linked by C-H⋯O inter-actions to form chains along the b axis.

摘要

在标题苯甲酰肼衍生物C₁₅H₁₄N₂O₂中,两个苯环平面之间的二面角为12.56 (9)°。偶氮甲碱双键采用E构型,通过N—H⋯O氢键得以稳定。在晶体中,各组分通过C—H⋯O相互作用沿b轴形成链状结构。

https://cdn.ncbi.nlm.nih.gov/pmc/blobs/c4d9/4186185/b4a393ee0e1e/e-70-o1071-fig1.jpg

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