Borges Boniek Castillo Dutra, Souza-Júnior Eduardo José, Catelan Anderson, Lovadino José Roberto, Dos Santos Paulo Henrique, Paulillo Luís Alexandre Maffei Sartini, Aguiar Flávio Henrique Baggio
Department of Restorative Dentistry, Piracicaba Dental School, State University of Campinas, Piracicaba, Brazil.
J Investig Clin Dent. 2010 Nov;1(2):151-5. doi: 10.1111/j.2041-1626.2010.00015.x.
To evaluate the conversion and plasticization of fissure sealer materials, as influenced by extended curing time.
Twenty specimens (n=5) of a pit and fissure sealant and a flowable composite at two curing times (20 and 60 sec) were photocured with the Bluephase 16i light-emitting diode. The conversion was determined by Fourier transform infrared/attenuated total reflection spectroscopy 24 h after polymerization. Hardness was measured, and samples were stored in absolute ethanol for 24 h. A second hardness measurement was executed after storage to assess plasticization by the percentage of hardness decrease. Data were analyzed by analysis of variance and Pearson's correlation (α=0.05).
The pit and fissure sealant showed lower degree of conversion than the flowable composite. The 60-sec curing time increased the conversion only for the flowable composite. Plasticization was lower for the flowable composite than for the pit and fissure sealant. The 60-sec light exposure time showed a similar percentage of hardness decrease of 20 sec. A low correlation between the conversion and plasticization was found.
Extended curing time improved the conversion only for the flowable composite. The pit and fissure sealant presented lower conversion and higher plasticization than the flowable composite.
评估延长固化时间对窝沟封闭剂材料转化率和增塑作用的影响。
采用Bluephase 16i发光二极管对20个样本(每种材料5个)的窝沟封闭剂和可流动复合树脂在两种固化时间(20秒和60秒)下进行光固化。聚合反应24小时后,通过傅里叶变换红外光谱/衰减全反射光谱法测定转化率。测量硬度,并将样本在无水乙醇中储存24小时。储存后再次测量硬度,以通过硬度降低百分比评估增塑作用。数据采用方差分析和Pearson相关性分析(α = 0.05)。
窝沟封闭剂的转化率低于可流动复合树脂。60秒的固化时间仅提高了可流动复合树脂的转化率。可流动复合树脂的增塑作用低于窝沟封闭剂。60秒的光照时间显示出与20秒相似的硬度降低百分比。发现转化率与增塑作用之间的相关性较低。
延长固化时间仅提高了可流动复合树脂的转化率。窝沟封闭剂的转化率低于可流动复合树脂,增塑作用高于可流动复合树脂。