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不同形貌银纳米颗粒的可控合成及其抗菌性能

Controlled synthesis of Ag nanoparticles with different morphologies and their antibacterial properties.

作者信息

Gao Minjie, Sun Lei, Wang Zhiqiang, Zhao Yanbao

机构信息

Key Laboratory for Special Functional Material of Ministry of Education, Henan University, Kaifeng 475004, PR China.

Key Laboratory for Special Functional Material of Ministry of Education, Henan University, Kaifeng 475004, PR China.

出版信息

Mater Sci Eng C Mater Biol Appl. 2013 Jan 1;33(1):397-404. doi: 10.1016/j.msec.2012.09.005. Epub 2012 Sep 23.

Abstract

In this paper, Ag triangle nanoplates and nanospheres were synthesized by liquid chemical reduction method in the presence of seeds, with L-ascorbic acid as the reductant and polyvinyl pyrrolidone (PVP) as the surface modification agent, respectively. Characterizations of the particles were conducted by various techniques such as X-ray powder diffraction, transmission electron microscopy, ultraviolet-visible absorption spectroscopy, Fourier transformation infrared spectrometry, and thermal analysis. The antibacterial properties of Ag nanoparticles against Escherichia coli, Staphylococcus aureus and Pseudomonas aeruginosa were investigated by disk diffusion and broth dilution methods. The results indicate that Ag nanospheres exhibit better antibacterial properties than that of triangle nanoplates.

摘要

本文分别以L-抗坏血酸为还原剂、聚乙烯吡咯烷酮(PVP)为表面改性剂,通过液相化学还原法在晶种存在的情况下合成了Ag三角形纳米片和纳米球。采用X射线粉末衍射、透射电子显微镜、紫外可见吸收光谱、傅里叶变换红外光谱和热分析等多种技术对颗粒进行了表征。通过纸片扩散法和肉汤稀释法研究了Ag纳米颗粒对大肠杆菌、金黄色葡萄球菌和铜绿假单胞菌的抗菌性能。结果表明,Ag纳米球比三角形纳米片表现出更好的抗菌性能。

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