Tamaki Y, Miyazaki T, Suzuki E, Miyaji T
Shika Zairyo Kikai. 1989 Jan;8(1):103-9.
Titanium was polished using several chemical polishing baths containing different ratios of hydrofluoric acid and nitric acid. The meltage, surface roughness, and surface texture of titanium samples after chemical polishing were affected by the ratio of hydrofluoric acid and nitric acid. Generally the meltage increased and surface roughness decreased when the mole concentration of hydrofluoric acid was high and that of nitric acid was low. For example the chemical polishing bath containing 5 mole hydrofluoric acid and 5 mole nitric acid improved the surface texture in one minute, but SEM observation revealed a partially rough surface caused by the excessive solution. The chemical polishing bath containing 1 mole hydrofluoric acid and 5 mole nitric acid did not improve the surface texture in a short time because of low solubility, but improved the surface texture gradually with the extension of the immersion time and a good surface texture was observed by SEM. The chemical polishing using the chemical polishing bath with low solubility and immersion of the prosthetics for a rather long time were considered useful procedures to obtain a smooth surface of titanium prosthetics while maintaining their accuracy.
使用含有不同比例氢氟酸和硝酸的几种化学抛光液对钛进行抛光。化学抛光后钛样品的熔蚀量、表面粗糙度和表面纹理受氢氟酸和硝酸比例的影响。一般来说,当氢氟酸的摩尔浓度高而硝酸的摩尔浓度低时,熔蚀量增加而表面粗糙度降低。例如,含有5摩尔氢氟酸和5摩尔硝酸的化学抛光液在一分钟内改善了表面纹理,但扫描电子显微镜观察显示,由于溶液过量导致表面部分粗糙。含有1摩尔氢氟酸和5摩尔硝酸的化学抛光液由于溶解度低,在短时间内没有改善表面纹理,但随着浸泡时间的延长逐渐改善了表面纹理,扫描电子显微镜观察到良好的表面纹理。使用低溶解度的化学抛光液进行化学抛光并将假体浸泡相当长的时间,被认为是在保持钛假体精度的同时获得光滑表面的有用方法。