Kara Ozlem, Kara Haluk Baris, Tobi Elif Sumeyye, Ozturk Atiye Nilgun, Kilic Hamdi Sukur
1 Department of Prosthodontics, BezmialemVakif University , Faculty of Dentistry, Istanbul, Turkey .
Photomed Laser Surg. 2015 Feb;33(2):69-76. doi: 10.1089/pho.2014.3841. Epub 2015 Feb 5.
The purpose of this study was to compare and evaluate the effects of various laser systems on surface roughness and shear bond strengths of zirconia ceramics.
Seventy-two ceramic discs (10 mm×2 mm) obtained from two sintered zirconia ceramics (Zirkonzahn, Zirkonzahn Prettau(®)) were divided into two groups (n=36) according to the computer-aided design (CAD)-computer-aided manufacturing (CAM) technique and then further divided into three groups (n=12). Each group was treated with one of the following: (1) femtosecond (FS), (2) Nd:YAG (NY), and (3) Er:YAG (EY) lasers. After laser irradiation, a scanning electron micrograph (SEM) was taken at 500× magnification for qualitative examination. Following surface roughness measurement by profilometry, resin cement (Rely X U200) was bonded to the ceramic specimens using Teflon tubes (3 mm height, 4 mm diameter). Specimens were stored in distilled water at 37°C for 24 h and then thermal cycled for 5000 cycles. A shear bond strength (MPa) test was performed using a universal testing machine at a crosshead speed of 1 mm/min. Data were analyzed by two way analysis of variance (ANOVA) and Tukey honest significant difference (HSD) tests for pairwise comparisons among groups (p=0.05).
MPa and roughness were significantly affected by laser type (p<0.001), and there was no significant interaction between the two zircon ceramics. The group irradiated with FS laser had significantly higher (p<0.05) roughness and MPa mean values than those of the other groups. No significant difference was found between the groups irradiated with NY and EY laser (p>0.05). In the SEM, the surfaces of the FS group were rougher than those of the NY and EY groups. NY and EY surfaces were nearly smooth.
FS laser is an effective surface treatment for roughening surfaces of zirconia ceramics. Furthermore, it reveals the highest MPa.
本研究旨在比较和评估不同激光系统对氧化锆陶瓷表面粗糙度和剪切粘结强度的影响。
从两种烧结氧化锆陶瓷(Zirkonzahn、Zirkonzahn Prettau(®))获得72个陶瓷圆盘(10毫米×2毫米),根据计算机辅助设计(CAD)-计算机辅助制造(CAM)技术分为两组(n = 36),然后进一步分为三组(n = 12)。每组分别用以下一种方法处理:(1)飞秒(FS)激光,(2)钕:钇铝石榴石(NY)激光,(3)铒:钇铝石榴石(EY)激光。激光照射后,以500倍放大倍数拍摄扫描电子显微镜照片(SEM)进行定性检查。通过轮廓仪测量表面粗糙度后,使用聚四氟乙烯管(高度3毫米,直径4毫米)将树脂粘结剂(Rely X U200)粘结到陶瓷试样上。试样在37°C蒸馏水中储存24小时,然后进行5000次热循环。使用万能试验机以1毫米/分钟的十字头速度进行剪切粘结强度(MPa)测试。数据通过双向方差分析(ANOVA)和Tukey诚实显著差异(HSD)检验进行分析,以进行组间两两比较(p = 0.05)。
MPa和粗糙度受激光类型显著影响(p < 0.001),两种氧化锆陶瓷之间无显著相互作用。FS激光照射组的粗糙度和MPa平均值显著高于其他组(p < 0.05)。NY激光和EY激光照射组之间未发现显著差异(p > 0.05)。在SEM中,FS组的表面比NY组和EY组更粗糙。NY组和EY组的表面几乎光滑。
FS激光是使氧化锆陶瓷表面粗糙化的有效表面处理方法。此外,它显示出最高的MPa。