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通过电子背散射衍射(EBSD)图像直接估算马氏体钢热影响区的奥氏体晶粒尺寸。

Direct estimation of austenitic grain dimensions in heat affected zones of a martensitic steel from EBSD images.

作者信息

Altendorf H, Faessel M, Jeulin D, Latourte F

机构信息

Centre of Mathematical Morphology, Mines Paris Tech, Fontainebleau cedex, France.

出版信息

J Microsc. 2015 May;258(2):87-104. doi: 10.1111/jmi.12210. Epub 2015 Feb 16.

DOI:10.1111/jmi.12210
PMID:25689129
Abstract

In the context of automated analyses of electron-backscattered-diffraction images, we present in this paper a novel method to automatically extract morphological properties of prior austenitic grains in martensitic steels based on raw crystallographic orientation maps. This quantification includes the estimation of the mean chord length in specific directions, with in addition the reconstruction of the mean shape of austenitic grains inducing anisotropic shape properties. The approach is based on the morphological measure of covariance on a decision curve of grain fidelity per disorientation angle. These efforts have been motivated by the need of realistic microstructures to perform micromechanical studies of grain boundary localized damage phenomenons in steels, one example being the type IV fracture phenomenon occurring in welded joints of grade P91/P92 steel. This failure is attributed to a change of the microstructure due to thermal gradients arising during the welding process. To precisely capture the relationships between microstructural changes and mechanical fields localization in a polycrystalline aggregate, we first need to achieve a reasonable stochastic model of its microstructure, which relies on a detailed knowledge of the microstructural morphology. As martensitic steels possess multiscale microstructures composed of prior austenitic grains, packets and laths, a relevant modelling strategy has to be proposed to account for the observed hierarchies. With this objective, this paper focuses on the larger scale entities present in the microstructure, namely, the austenitic grains.

摘要

在电子背散射衍射图像自动分析的背景下,我们在本文中提出了一种基于原始晶体取向图自动提取马氏体钢中原始奥氏体晶粒形态特征的新方法。这种量化包括估计特定方向上的平均弦长,此外还包括重建具有各向异性形状特征的奥氏体晶粒的平均形状。该方法基于每个取向差角度的晶粒保真度决策曲线上的协方差形态测量。这些工作的动机是需要真实的微观结构来对钢中晶界局部损伤现象进行微观力学研究,一个例子是P91/P92钢焊接接头中出现的IV型断裂现象。这种失效归因于焊接过程中由于热梯度引起的微观结构变化。为了精确捕捉多晶聚集体中微观结构变化与机械场局部化之间的关系,我们首先需要建立一个合理的微观结构随机模型,这依赖于对微观结构形态的详细了解。由于马氏体钢具有由原始奥氏体晶粒、晶包和板条组成的多尺度微观结构,因此必须提出一种相关的建模策略来考虑观察到的层次结构。出于这个目的,本文关注微观结构中存在的较大尺度实体,即奥氏体晶粒。

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