Park Sung-Hyeon, Kim Hak-Sung
School of Mechanical Engineering, Hanyang University, 17 Haengdang-dong, Seongdong-gu, Seoul 133-791, Korea.
Nanotechnology. 2015 May 22;26(20):205601. doi: 10.1088/0957-4484/26/20/205601. Epub 2015 Apr 27.
In this work, we demonstrate an environmentally benign and facile flash light irradiation process to reduce graphene oxide (GO). GO thin films were prepared by a vacuum filtration process, and these films were reduced by exposure to flash light irradiation for a few milliseconds at room temperature under ambient conditions. Flash light conditions such as energy, pulse width, and pulse number were varied to determine optimal conditions for this photothermal reduction of GO. The flash light irradiation treatment completely reduced the GO thin films, transforming them into pure graphene films. The resulting graphene films were characterized by x-ray diffraction, x-ray photoelectron spectroscopy, Raman spectroscopy, transmission electron microscopy, and thermogravimetric analysis.
在本工作中,我们展示了一种环境友好且简便的闪光照射工艺来还原氧化石墨烯(GO)。通过真空过滤工艺制备了GO薄膜,在室温及环境条件下,将这些薄膜暴露于闪光照射下几毫秒进行还原。改变诸如能量、脉冲宽度和脉冲数等闪光条件,以确定这种GO光热还原的最佳条件。闪光照射处理完全还原了GO薄膜,将它们转化为纯石墨烯薄膜。通过X射线衍射、X射线光电子能谱、拉曼光谱、透射电子显微镜和热重分析对所得的石墨烯薄膜进行了表征。