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使用传统茚三酮和1,2-茚二酮在热敏纸上显现潜指纹

Latent Fingerprint Development on Thermal Paper Using Traditional Ninhydrin and 1,2-indanedione.

作者信息

Chen Chun-Chieh, Yu Yung-Chien, Lee Henry C, Giang Yun-Seng, Wang Sheng-Meng

机构信息

Forensic Science Section, Changhua County Police Bureau, 778, Sec. 2, Jhong-jheng Rd., Changhua City, 50004, Taiwan.

Department of Forensic Science, Central Police University, 56, Shu-Jen Road, Kwei-San, Taoyuan, 33304, Taiwan.

出版信息

J Forensic Sci. 2016 Jan;61(1):219-25. doi: 10.1111/1556-4029.12897. Epub 2015 Aug 6.

Abstract

Thermal paper poses a significant challenge to latent print development as it tends to change color when traditional fingerprint development formulations are applied to it. In this study, the optimal components of ninhydrin, 1,2-indanedione, 1,8-diazafluoren-9-one (DFO), and 5-methylthioninhydrin (5-MTN) for yielding clear fingerprints on thermal paper were determined by systematically adjusting the relative amounts of the reagents, polar solvents, and the nonpolar diluent petroleum ether, followed by validation on text-printed thermal paper. Specifically, 3.0% ethyl acetate as the polar solvent in petroleum ether was found to be the optimal combination; the optimal dilution ratios of ninhydrin, DFO, and 5-MTN original solutions with petroleum ether were 1 to 2, 11, and 7, respectively. The optimal concentration of 1,2-indanedione in petroleum ether was 0.125 g/L, with a string of 0.5% ethyl acetate in petroleum ether.

摘要

热敏纸对潜在指纹显现有重大挑战,因为当将传统指纹显影配方应用于热敏纸时,它往往会变色。在本研究中,通过系统地调整试剂、极性溶剂和非极性稀释剂石油醚的相对用量,确定了茚三酮、1,2-茚二酮、1,8-二氮杂芴-9-酮(DFO)和5-甲基硫代茚三酮(5-MTN)在热敏纸上产生清晰指纹的最佳成分,随后在文本打印的热敏纸上进行了验证。具体而言,发现石油醚中3.0%的乙酸乙酯作为极性溶剂是最佳组合;茚三酮、DFO和5-MTN原液与石油醚的最佳稀释比例分别为1比2、11和7。石油醚中1,2-茚二酮的最佳浓度为0.125 g/L,石油醚中乙酸乙酯的含量为0.5%。

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