Chen Wei, Qin Shiqiao, Zhang Xue-Ao, Fang Jingyue, Wang Guang, Zhang Sen, Wang Chaocheng, Wang Li, Chang Shengli
J Nanosci Nanotechnol. 2015 Jun;15(6):4591-5. doi: 10.1166/jnn.2015.9782.
The graphene, as a one atomic-layer material, is very sensitive to the environment and easy to be polluted. Here, we propose an in situ fabrication and characterization method for graphene electronic devices using the Dual Beam system. Instead of the conventional photo/e-beam lithography, plasma etching and lift-off techniques, the focused ion beam (FIB) is employed to pattern the graphene and the e-beam induced deposition of platinum (Pt) is adopted to fabricate the electrodes. Using the nano-probes in the specimen chamber, we obtained the typical electronic bipolar behavior of graphene in situ both with the Pt/graphene contact and the nano-probes/graphene direct contact. In the whole process of the fabrication and characterization, the graphene sample is kept in high vacuum condition all the time.
作为一种单原子层材料,石墨烯对环境非常敏感且容易被污染。在此,我们提出一种使用双束系统对石墨烯电子器件进行原位制备和表征的方法。与传统的光/电子束光刻、等离子体蚀刻和剥离技术不同,我们采用聚焦离子束(FIB)对石墨烯进行图案化,并采用电子束诱导铂(Pt)沉积来制造电极。利用样品室中的纳米探针,我们在Pt/石墨烯接触以及纳米探针/石墨烯直接接触的情况下原位获得了石墨烯典型的电子双极行为。在制备和表征的整个过程中,石墨烯样品始终保持在高真空条件下。