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用于利用高能同步辐射对薄膜生长进行原位X射线衍射研究的与工业相关的磁控溅射和阴极电弧超高真空沉积系统。

Industry-relevant magnetron sputtering and cathodic arc ultra-high vacuum deposition system for in situ x-ray diffraction studies of thin film growth using high energy synchrotron radiation.

作者信息

Schroeder J L, Thomson W, Howard B, Schell N, Näslund L-Å, Rogström L, Johansson-Jõesaar M P, Ghafoor N, Odén M, Nothnagel E, Shepard A, Greer J, Birch J

机构信息

Department of Physics, Chemistry, and Biology (IFM), Linköping University, SE-581 83 Linköping, Sweden.

PVD Products Inc., 35 Upton Dr., Suite 200, Wilmington, Massachusetts 01887, USA.

出版信息

Rev Sci Instrum. 2015 Sep;86(9):095113. doi: 10.1063/1.4930243.

Abstract

We present an industry-relevant, large-scale, ultra-high vacuum (UHV) magnetron sputtering and cathodic arc deposition system purposefully designed for time-resolved in situ thin film deposition/annealing studies using high-energy (>50 keV), high photon flux (>10(12) ph/s) synchrotron radiation. The high photon flux, combined with a fast-acquisition-time (<1 s) two-dimensional (2D) detector, permits time-resolved in situ structural analysis of thin film formation processes. The high-energy synchrotron-radiation based x-rays result in small scattering angles (<11°), allowing large areas of reciprocal space to be imaged with a 2D detector. The system has been designed for use on the 1-tonne, ultra-high load, high-resolution hexapod at the P07 High Energy Materials Science beamline at PETRA III at the Deutsches Elektronen-Synchrotron in Hamburg, Germany. The deposition system includes standard features of a typical UHV deposition system plus a range of special features suited for synchrotron radiation studies and industry-relevant processes. We openly encourage the materials research community to contact us for collaborative opportunities using this unique and versatile scientific instrument.

摘要

我们展示了一种与工业相关的大规模超高真空(UHV)磁控溅射和阴极电弧沉积系统,该系统专为使用高能(>50 keV)、高光子通量(>10¹² ph/s)同步辐射进行时间分辨原位薄膜沉积/退火研究而设计。高光子通量与快速采集时间(<1 s)的二维(2D)探测器相结合,能够对薄膜形成过程进行时间分辨原位结构分析。基于高能同步辐射的X射线产生小散射角(<11°),使得二维探测器能够对倒易空间的大面积区域进行成像。该系统设计用于德国汉堡的德国电子同步加速器PETRA III的P07高能材料科学光束线上的1吨超高负载、高分辨率六轴平台。该沉积系统具备典型超高真空沉积系统的标准特性,还拥有一系列适用于同步辐射研究和与工业相关工艺的特殊特性。我们诚挚地鼓励材料研究界与我们联系,以利用这一独特且多功能的科学仪器开展合作。

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