Department of Chemistry, University of North Texas , Denton, Texas 76203, United States.
Inficon , Syracuse, New York 13057, United States.
Anal Chem. 2015 Nov 17;87(22):11501-8. doi: 10.1021/acs.analchem.5b03269. Epub 2015 Oct 27.
The ability to detect atmospheric effluent from clandestine methamphetamine manufacture is a useful tool for law enforcement. A membrane inlet mass spectrometer is mounted onto an all-electric drive capable hybrid vehicle that samples the atmosphere while in motion. Attributing a latitude and longitude to each spectrum collected, unique chemical fingerprints from clandestine manufacture are then mapped. This location-based mass spectrum data provides a localization to an area of interest. The synthesis of methamphetamine precursors was performed, and the impurities from such reactions were observed. A mock manufacture was setup, and the impurities were introduced into the atmosphere via heating. The detection of products and impurities using this mobile platform has shown the effectiveness of locating and localizing the manufacture of methamphetamine.
检测秘密制造冰毒的大气流出物的能力是执法的有用工具。将膜进样质谱仪安装在能够进行采样的全电动驱动混合动力汽车上,使其能够在运动中对大气进行采样。为采集到的每个光谱赋予一个经纬度,然后对来自秘密制造的独特化学指纹进行绘制。这种基于位置的质谱数据提供了对感兴趣区域的定位。进行了冰毒前体的合成,并观察了此类反应的杂质。建立了一个模拟制造,并通过加热将杂质引入大气中。使用这个移动平台检测产物和杂质表明了定位和定位冰毒制造的有效性。