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新型纤维增强复合材料与大块充填复合材料力学性能的比较。

Comparison of mechanical properties of a new fiber reinforced composite and bulk filling composites.

作者信息

Abouelleil Hazem, Pradelle Nelly, Villat Cyril, Attik Nina, Colon Pierre, Grosgogeat Brigitte

机构信息

Laboratoire des Multimatériaux et Interfaces, UMR CNRS 5615, Université Lyon1, Villeurbanne, France.

Laboratoire des Multimatériaux et Interfaces, UMR CNRS 5615, Université Lyon1, Villeurbanne, France. ; UFR D'odontologie, Université Paris Diderot, APHP, Hôpital Rothschild, Service d'Odontologie, Paris, France.

出版信息

Restor Dent Endod. 2015 Nov;40(4):262-70. doi: 10.5395/rde.2015.40.4.262. Epub 2015 Sep 2.

Abstract

OBJECTIVES

The aim of this study was to evaluate the mechanical and physical properties of a newly developed fiber reinforced dental composite.

MATERIALS AND METHODS

Fiber reinforced composite EverX Posterior (EXP, GC EUROPE), and other commercially available bulk fill composites, including Filtek Bulk Fill (FB, 3M ESPE), SonicFill (SF, Kerr Corp.), SureFil (SDR, Dentsply), Venus Bulk Fill (VB, HerausKultzer), Tetric evoceram bulk fill (TECB, Ivoclar Vivadent), and Xtra Base (XB, Voco) were characterized. Composite samples light-cured with a LED device were evaluated in terms of flexural strength, flexural modulus (ISO 4049, n = 6), fracture toughness (n = 6), and Vickers hardness (0, 2, and 4 mm in depth at 24 hr, n = 5). The EXP samples and the fracture surface were observed under a scanning electron microscopy. Data were statistically analyzed using one-way ANOVA and unpaired t-test.

RESULTS

EXP, FB, and VB had significantly higher fracture toughness value compared to all the other bulk composite types. SF, EXP, and XB were not statistically different, and had significantly higher flexural strength values compared to other tested composite materials. EXP had the highest flexural modulus, VB had the lowest values. Vickers hardness values revealed SF, EXP, TECB, and XB were not statistically different, and had significantly higher values compared to other tested composite materials. SEM observations show well dispersed fibers working as a reinforcing phase.

CONCLUSIONS

The addition of fibers to methacrylate-based matrix results in composites with either comparable or superior mechanical properties compared to the other bulk fill materials tested.

摘要

目的

本研究旨在评估一种新开发的纤维增强牙科复合材料的力学和物理性能。

材料与方法

对纤维增强复合材料EverX Posterior(EXP,GC欧洲公司)以及其他市售的大块充填复合材料进行了表征,这些复合材料包括Filtek Bulk Fill(FB,3M ESPE公司)、SonicFill(SF, Kerr公司)、SureFil(SDR,登士柏公司)、Venus Bulk Fill(VB,贺利氏古莎公司)、Tetric evoceram bulk fill(TECB,义获嘉伟瓦登特公司)和Xtra Base(XB,VOCO公司)。使用LED设备光固化的复合材料样本,根据弯曲强度、弯曲模量(ISO 4049,n = 6)、断裂韧性(n = 6)和维氏硬度(24小时时深度为0、2和4毫米,n = 5)进行评估。在扫描电子显微镜下观察EXP样本和断裂表面。使用单因素方差分析和非配对t检验对数据进行统计分析。

结果

与所有其他大块复合材料类型相比,EXP、FB和VB具有显著更高的断裂韧性值。SF、EXP和XB在统计学上没有差异,并且与其他测试的复合材料相比具有显著更高的弯曲强度值。EXP具有最高的弯曲模量,VB具有最低的值。维氏硬度值显示SF、EXP、TECB和XB在统计学上没有差异,并且与其他测试的复合材料相比具有显著更高的值。扫描电子显微镜观察表明,纤维分散良好,起到增强相的作用。

结论

与其他测试的大块充填材料相比,在甲基丙烯酸酯基基质中添加纤维可使复合材料具有相当或更优异的力学性能。

https://cdn.ncbi.nlm.nih.gov/pmc/blobs/f500/4650521/ff7f15abf52c/rde-40-262-g001.jpg

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