Department of Biomaterials Science and Turku Clinical Biomaterial Center-TCBC, Institute of Dentistry, University of Turku, Turku, Finland.
Research Development and Production Department, Stick Tech Ltd-Member of GC Group, Turku, Finland.
Odontology. 2019 Jul;107(3):342-352. doi: 10.1007/s10266-018-0405-y. Epub 2019 Jan 8.
This study aimed to evaluate certain physical properties including surface wear of a new experimental short fiber-reinforced flowable resin composite (SFRC) in comparison with different commercial flowable bulk fill resin composites (SDR, Tetric EvoFlow Bulk Fill, Filtek Bulk Fill Flowable and Estelite Bulk Fill Flow). The following properties were examined according to ISO standard: flexural strength, flexural modulus, fracture toughness, water sorption, volumetric shrinkage, and depth of cure. Degree of conversion (DC%) was determined by FTIR spectrometry. A wear test was conducted with 15000 chewing cycles using a dual-axis chewing simulator. Wear depth was measured by a three-dimensional (3D) noncontact optical profilometer. Scanning electron microscopy was used to evaluate the microstructure of SFRC. Data were statistically analyzed with analysis of variance ANOVA (p = 0.05). SFRC exhibited the highest fracture toughness (2.8 MPa m) and flexural strength (146.5 MPa) values (p < 0.05) and the greatest depth of cure (5 mm) and lowest wear depth (18.2 µm) among the flowable bulk fill materials tested. SDR showed the lowest volumetric shrinkage percentage (2.9%), while the other resin composites had comparable volumetric shrinkage values (p > 0.05). The new short fiber-reinforced flowable resin composite differed significantly in its measured fracture toughness compared to the tested flowable bulk fill resin composites.
本研究旨在评估一种新型短纤维增强型流动树脂复合材料(SFRC)的某些物理性能,包括表面磨损情况,并与不同的商业流动型大体积充填树脂复合材料(SDR、Tetric EvoFlow Bulk Fill、Filtek Bulk Fill Flowable 和 Estelite Bulk Fill Flow)进行比较。根据 ISO 标准,对以下性能进行了检查:弯曲强度、弯曲模量、断裂韧性、吸水率、体积收缩率和固化深度。通过傅里叶变换红外光谱法(FTIR)测定转化率(DC%)。采用双轴咀嚼模拟器进行了 15000 次咀嚼循环的磨损试验。使用三维(3D)非接触光学轮廓仪测量磨损深度。扫描电子显微镜用于评估 SFRC 的微观结构。采用方差分析(ANOVA)进行数据统计分析(p=0.05)。SFRC 表现出最高的断裂韧性(2.8 MPa m)和弯曲强度(146.5 MPa)值(p<0.05),以及最大的固化深度(5 mm)和最低的磨损深度(18.2 µm),在测试的流动大体积充填材料中。SDR 的体积收缩率最低(2.9%),而其他树脂复合材料的体积收缩率相当(p>0.05)。与测试的流动大体积充填树脂复合材料相比,新型短纤维增强型流动树脂复合材料的断裂韧性有显著差异。