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ID16B:欧洲同步辐射装置上用于纳米分析的硬X射线纳米探针光束线。

ID16B: a hard X-ray nanoprobe beamline at the ESRF for nano-analysis.

作者信息

Martínez-Criado Gema, Villanova Julie, Tucoulou Rémi, Salomon Damien, Suuronen Jussi-Petteri, Labouré Sylvain, Guilloud Cyril, Valls Valentin, Barrett Raymond, Gagliardini Eric, Dabin Yves, Baker Robert, Bohic Sylvain, Cohen Cédric, Morse John

机构信息

European Synchrotron Radiation Facility, 71 Avenue des Martyrs, 38000 Grenoble, France.

出版信息

J Synchrotron Radiat. 2016 Jan;23(1):344-52. doi: 10.1107/S1600577515019839. Epub 2016 Jan 1.

Abstract

Within the framework of the ESRF Phase I Upgrade Programme, a new state-of-the-art synchrotron beamline ID16B has been recently developed for hard X-ray nano-analysis. The construction of ID16B was driven by research areas with major scientific and societal impact such as nanotechnology, earth and environmental sciences, and bio-medical research. Based on a canted undulator source, this long beamline provides hard X-ray nanobeams optimized mainly for spectroscopic applications, including the combination of X-ray fluorescence, X-ray diffraction, X-ray excited optical luminescence, X-ray absorption spectroscopy and 2D/3D X-ray imaging techniques. Its end-station re-uses part of the apparatus of the earlier ID22 beamline, while improving and enlarging the spectroscopic capabilities: for example, the experimental arrangement offers improved lateral spatial resolution (∼50 nm), a larger and more flexible capability for in situ experiments, and monochromatic nanobeams tunable over a wider energy range which now includes the hard X-ray regime (5-70 keV). This paper describes the characteristics of this new facility, short-term technical developments and the first scientific results.

摘要

在欧洲同步辐射装置(ESRF)一期升级计划的框架内,最近开发了一条用于硬X射线纳米分析的全新先进同步辐射光束线ID16B。ID16B的建设是由纳米技术、地球与环境科学以及生物医学研究等具有重大科学和社会影响的研究领域推动的。基于倾斜波荡器源,这条长光束线提供主要针对光谱应用优化的硬X射线纳米束,包括X射线荧光、X射线衍射、X射线激发光致发光、X射线吸收光谱以及二维/三维X射线成像技术的组合。其实验终端复用了早期ID22光束线的部分设备,同时提升并扩展了光谱分析能力:例如,实验装置提供了更高的横向空间分辨率(约50纳米)、更强的原位实验能力以及更大的灵活性,并且单色纳米束的能量范围更宽,现在涵盖了硬X射线区域(5 - 70千电子伏特)。本文描述了这个新设施的特点、短期技术发展以及首批科学成果。

https://cdn.ncbi.nlm.nih.gov/pmc/blobs/ef66/5297598/9b0a1dbb8c6c/s-23-00344-fig1.jpg

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