Quinn Paul D, Alianelli Lucia, Gomez-Gonzalez Miguel, Mahoney David, Cacho-Nerin Fernando, Peach Andrew, Parker Julia E
Diamond Light Source, Harwell Science and Innovation Campus, Didcot, Oxfordshire OX11 0DE, United Kingdom.
J Synchrotron Radiat. 2021 May 1;28(Pt 3):1006-1013. doi: 10.1107/S1600577521002502. Epub 2021 Apr 9.
The Hard X-ray Nanoprobe beamline, I14, at Diamond Light Source is a new facility for nanoscale microscopy. The beamline was designed with an emphasis on multi-modal analysis, providing elemental mapping, speciation mapping by XANES, structural phase mapping using nano-XRD and imaging through differential phase contrast and ptychography. The 185 m-long beamline operates over a 5 keV to 23 keV energy range providing a ≤50 nm beam size for routine user experiments and a flexible scanning system allowing fast acquisition. The beamline achieves robust and stable operation by imaging the source in the vertical direction and implementing horizontally deflecting primary optics and an overfilled secondary source in the horizontal direction. This paper describes the design considerations, optical layout, aspects of the hardware engineering and scanning system in operation as well as some examples illustrating the beamline performance.
位于英国钻石光源(Diamond Light Source)的硬X射线纳米探针光束线I14是一种用于纳米级显微镜观察的新型设备。该光束线的设计重点是多模态分析,可提供元素映射、通过X射线吸收近边结构(XANES)进行的物种映射、使用纳米X射线衍射(nano-XRD)进行的结构相映射以及通过差分相衬和叠层成像进行的成像。这条185米长的光束线在5千电子伏特至23千电子伏特的能量范围内运行,为常规用户实验提供≤50纳米的光束尺寸,并配备灵活的扫描系统,能够快速采集数据。该光束线通过在垂直方向对光源成像,并在水平方向采用水平偏转的一次光学元件和过填充的二次光源,实现了稳定可靠的运行。本文介绍了设计考量、光学布局、硬件工程方面以及运行中的扫描系统,还列举了一些说明该光束线性能的实例。