Raghavendra Gownolla Malegowd, Jung Jeyoung, Kim Dowan, Seo Jongchul
Department of Packaging, Yonsei University, Kangwondo 220-710, Republic of Korea.
Department of Packaging, Yonsei University, Kangwondo 220-710, Republic of Korea.
Int J Biol Macromol. 2016 Mar;84:281-8. doi: 10.1016/j.ijbiomac.2015.12.026. Epub 2015 Dec 17.
In the current approach, antibacterial chitosan-silver nanocomposite films were fabricated through microwave irradiation. During the process, by utilizing chitosan as reducing agent, silver nanoparticles were synthesized within 11 min by microwave irradiation. Further, films were fabricated within 90 min. It involved an energy consumption of just 0.146 kWh to synthesize silver nanoparticles. This is many times less than the energy consumed during conventional methods. The silver nanoparticles were examined through UV-vis spectrum and transmission electron microscopy (TEM). The fabricated films were characterized by using scanning electron microscopy coupled with an energy dispersive spectrometer (SEM-EDS), Fourier transform infrared spectroscopy (FTIR), thermogravimetric analysis (TGA), and contact angle (CA) measurements. The films exhibited antibacterial properties against both Gram-negative micro-organisms (Escherichia coli; E. coli) and Gram-positive micro-organisms (Staphylococcus aureus; S. aureus). In overall, the procedure adopted for fabricating these antibacterial films is environmental friendly, time-saving and energy-saving.
在当前方法中,通过微波辐射制备了抗菌壳聚糖-银纳米复合薄膜。在此过程中,利用壳聚糖作为还原剂,通过微波辐射在11分钟内合成了银纳米颗粒。此外,在90分钟内制备了薄膜。合成银纳米颗粒仅消耗0.146千瓦时的能量。这比传统方法消耗的能量少很多倍。通过紫外-可见光谱和透射电子显微镜(TEM)对银纳米颗粒进行了检测。使用扫描电子显微镜结合能量色散光谱仪(SEM-EDS)、傅里叶变换红外光谱(FTIR)、热重分析(TGA)和接触角(CA)测量对制备的薄膜进行了表征。这些薄膜对革兰氏阴性微生物(大肠杆菌;E. coli)和革兰氏阳性微生物(金黄色葡萄球菌;S. aureus)均表现出抗菌性能。总体而言,制备这些抗菌薄膜所采用的方法是环保、省时且节能的。