Umar Ahmad
J Nanosci Nanotechnol. 2015 Sep;15(9):6704-9. doi: 10.1166/jnn.2015.10754.
This paper reports the successful fabrication and characterization of phenyl hydrazine chemical sensor based on CuO rosette-like nanostructures. The CuO rosette-like nanostructures were synthesized by facile hydrothermal process at low-temperature and characterized in detail in terms of their morphological, structural and compositional properties. The detailed morphological studies revealed that the prepared CuO rosettes are made by the accumulation of hundreds of small CuO nanodisks which are arranged in a special fashion that they made rosette-like morphologies. The structural characterization, by X-ray diffraction (XRD), confirmed that the prepared CuO rosette-like structures are nanocrystalline and possessing monoclinic structure. The compositional studies further substantiates that the synthesized rosette-like morphologies are pure CuO. The fabricated phenyl hydrazine chemical sensor based on CuO rosette-like nanostructures exhibited very high sensitivity of -49.532710 μA/cm2 x mM. Due to high sensitivity, it can be concluded that CuO rosette-like nanostructures could be an effective candidate for the fabrication of highly sensitive phenyl hydrazine chemical sensors.
本文报道了基于氧化铜玫瑰花状纳米结构的苯肼化学传感器的成功制备与表征。氧化铜玫瑰花状纳米结构通过简便的低温水热法合成,并对其形态、结构和组成性质进行了详细表征。详细的形态学研究表明,制备的氧化铜玫瑰花是由数百个小的氧化铜纳米盘堆积而成,这些纳米盘以特殊的方式排列形成玫瑰花状形态。通过X射线衍射(XRD)进行的结构表征证实,制备的氧化铜玫瑰花状结构是纳米晶,具有单斜结构。组成研究进一步证实,合成的玫瑰花状形态是纯氧化铜。基于氧化铜玫瑰花状纳米结构制备的苯肼化学传感器表现出非常高的灵敏度,为-49.532710 μA/cm2 x mM。由于高灵敏度,可以得出结论,氧化铜玫瑰花状纳米结构可能是制备高灵敏度苯肼化学传感器的有效候选材料。