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光学溶胶-凝胶薄膜的表面声波表征

Surface acoustic wave characterization of optical sol-gel thin layers.

作者信息

Fall Dame, Compoint François, Duquennoy Marc, Piombini Hervé, Ouaftouh Mohammadi, Jenot Frédéric, Piwakowski Bogdan, Belleville Philippe, Ambard Chrystel

机构信息

IEMN-DOAE (UMR CNRS 8520), Institut d'Electronique, de Microélectronique et de Nanotechnologie, Département d'Opto-Acousto-Electronique, Université de Valenciennes, 59313 Valenciennes, France.

CEA, DAM, Le Ripault, F-37260 Monts, France.

出版信息

Ultrasonics. 2016 May;68:102-7. doi: 10.1016/j.ultras.2016.02.006. Epub 2016 Feb 13.

DOI:10.1016/j.ultras.2016.02.006
PMID:26930248
Abstract

Controlling the thin film deposition and mechanical properties of materials is a major challenge in several fields of application. We are more particularly interested in the characterization of optical thin layers produced using sol-gel processes to reduce laser-induced damage. The mechanical properties of these coatings must be known to control and maintain optimal performance under various solicitations during their lifetime. It is therefore necessary to have means of characterization adapted to the scale and nature of the deposited materials. In this context, the dispersion of ultrasonic surface waves induced by a micrometric layer was studied on an amorphous substrate (fused silica) coated with a layer of ormosil using a sol-gel process. Our ormosil material is a silica-PDMS mixture with a variable polydimethylsiloxane (PDMS) content. The design and implementation of Surface Acoustic Wave InterDigital Transducers (SAW-IDT) have enabled quasi-monochromatic Rayleigh-type SAW to be generated and the dispersion phenomenon to be studied over a wide frequency range. Young's modulus and Poisson's ratio of coatings were estimated using an inverse method.

摘要

控制材料的薄膜沉积和机械性能是多个应用领域面临的重大挑战。我们尤其关注使用溶胶 - 凝胶工艺制备的光学薄膜的特性,以减少激光诱导损伤。必须了解这些涂层的机械性能,以便在其使用寿命期间的各种作用下控制并维持最佳性能。因此,需要有适合所沉积材料的规模和性质的表征方法。在此背景下,利用溶胶 - 凝胶工艺在涂覆有一层有机硅氧烷的非晶衬底(熔融石英)上研究了由微米级层引起的超声表面波的色散。我们的有机硅氧烷材料是一种二氧化硅 - 聚二甲基硅氧烷混合物,其聚二甲基硅氧烷(PDMS)含量可变。表面声波叉指换能器(SAW-IDT)的设计与实现使得能够产生准单色瑞利型表面声波,并在很宽的频率范围内研究色散现象。使用反演方法估算了涂层的杨氏模量和泊松比。

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