Hanifehpour Younes, Safarifard Vahid, Morsali Ali, Mirtamizdoust Babak, Joo Sang Woo
School of Mechanical Engineering, Yeungnam University, Gyongsan 712-749, South Korea.
Department of Chemistry, Faculty of Sciences, Tarbiat Modares University, P.O. Box 14115-4838, Tehran, Islamic Republic of Iran.
Ultrason Sonochem. 2016 Jul;31:201-5. doi: 10.1016/j.ultsonch.2015.12.020. Epub 2015 Dec 30.
High-energy ultrasound irradiation has been used for the synthesis of a new copper(II) coordination supramolecular compound, Cu2(μ-O2CCH3)2(μ-OOCCH3)(phen)2 (1), ("phen" is 1,10-phenanthroline) with nano-rods morphology. The new nano-structure was characterized by scanning electron microscopy (SEM), X-ray powder diffraction (XRPD), FT-IR spectroscopy and elemental analyses. Compound 1 was structurally characterized by single crystal X-ray diffraction. The utilization of high intensity ultrasound has found as a facile, environmentally friendly, and versatile synthetic tool for the supramolecular coordination compounds.
高能超声辐照已被用于合成一种具有纳米棒形态的新型铜（II）配位超分子化合物Cu2(μ-O2CCH3)2(μ-OOCCH3)(phen)2（1），（“phen”为1,10-菲咯啉）。通过扫描电子显微镜（SEM）、X射线粉末衍射（XRPD）、傅里叶变换红外光谱（FT-IR）和元素分析对这种新的纳米结构进行了表征。化合物1通过单晶X射线衍射进行了结构表征。高强度超声的应用已成为一种用于超分子配位化合物的简便、环保且通用的合成工具。
