Fekri Leila Zare, Fard Hajar Saeedi
Acta Chim Slov. 2016;63(2):263-70. doi: 10.17344/acsi.2015.2096.
A general synthetic route to dibenzoxanthenes has been developed using 1,4-diazaniumbicyclo[2.2.2]octane diacetate as a new bis ionic liquid under thermal and solvent free condition. This method provides several advantages such as a simple work-up, environmental friendliness and shorter reaction time along with high yields. All of the synthesized compounds were characterized by infrared spectroscopy, 1H and 13C spectroscopy and elemental analyses.
已经开发出一种通用的二苯并氧杂蒽合成路线,该路线使用1,4 - 二氮杂双环[2.2.2]辛烷二乙酸盐作为一种新型双离子液体,在无热和无溶剂条件下进行反应。该方法具有诸多优点,如后处理简单、环境友好、反应时间短以及产率高。所有合成的化合物均通过红外光谱、¹H和¹³C光谱以及元素分析进行了表征。