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水热老化后整体式和核芯氧化锆的透明度

Translucency of monolithic and core zirconia after hydrothermal aging.

作者信息

Fathy Salma M, El-Fallal Abeer A, El-Negoly Salwa A, El Bedawy Abu Baker

机构信息

Department of Dental Biomaterial, Faculty of Dentistry, Mansura University , Mansoura , Egypt.

Department of Physics, Faculty of Science, Mansura University , Mansoura , Egypt.

出版信息

Acta Biomater Odontol Scand. 2015 Dec 23;1(2-4):86-92. doi: 10.3109/23337931.2015.1102639. Epub 2015 Nov 9.

DOI:10.3109/23337931.2015.1102639
PMID:27335897
原文链接:https://pmc.ncbi.nlm.nih.gov/articles/PMC4894082/
Abstract

: To evaluate the hydrothermal aging effect on the translucency of partially stabilized tetragonal zirconia with yttria (Y-TZP) used as monolithic or fully milled zirconia and of core type. : Twenty disc-shaped specimens (1 and 10 mm) for each type of monolithic and core Y-TZP materials were milled and sintered according to the manufacturer's instruction. The final specimens were divided into two groups according to the type of Y-TZP used. Translucency parameter (TP) was measured over white and black backgrounds with the diffuse reflectance method; X-ray diffraction (XRD) and scanning electron microscope (SEM) were used to analyze the microstructure of both Y-TZP types before and after aging. Data for TP values was statistically analyzed using Student's -test. : Monolithic Y-TZP showed the highest TP mean value (16.4 ± 0.316) before aging while core Y-TZP showed the lowest TP mean value (7.05 ± 0.261) after aging. There was a significant difference between the two Y-TZP types before and after hydrothermal aging. XRD analysis showed increases in monoclinic content in both Y-TZP surfaces after aging. : Monolithic Y-TZP has a higher chance to low-temperature degradation than core type, which may significantly affect the esthetic appearance and translucency hence durability of translucent Y-TZP.

摘要

评估水热老化对用作整体式或全研磨氧化锆且为核型的部分稳定四方氧化钇锆(Y-TZP)的透明度的影响。:按照制造商的说明对每种整体式和核型Y-TZP材料研磨并烧结20个圆盘形试样(1毫米和10毫米)。最终试样根据所用Y-TZP的类型分为两组。使用漫反射法在白色和黑色背景上测量透明度参数(TP);使用X射线衍射(XRD)和扫描电子显微镜(SEM)分析老化前后两种Y-TZP类型的微观结构。使用学生t检验对TP值数据进行统计分析。:整体式Y-TZP在老化前显示出最高的TP平均值(16.4±0.316),而核型Y-TZP在老化后显示出最低的TP平均值(7.05±0.261)。在水热老化前后,两种Y-TZP类型之间存在显著差异。XRD分析表明,老化后两种Y-TZP表面的单斜晶含量均增加。:整体式Y-TZP比核型更容易发生低温降解,这可能会显著影响半透明Y-TZP的美学外观、透明度以及耐久性。

https://cdn.ncbi.nlm.nih.gov/pmc/blobs/fadc/5433221/1db189b5045f/iabo_a_1102639_f0004_c.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/fadc/5433221/90140ca2704d/iabo_a_1102639_f0001_c.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/fadc/5433221/a1f06ca4457b/iabo_a_1102639_f0002_c.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/fadc/5433221/d3b0d3d2c38c/iabo_a_1102639_f0003_b.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/fadc/5433221/1db189b5045f/iabo_a_1102639_f0004_c.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/fadc/5433221/90140ca2704d/iabo_a_1102639_f0001_c.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/fadc/5433221/a1f06ca4457b/iabo_a_1102639_f0002_c.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/fadc/5433221/d3b0d3d2c38c/iabo_a_1102639_f0003_b.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/fadc/5433221/1db189b5045f/iabo_a_1102639_f0004_c.jpg

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Direct evidence for continuous linear kinetics in the low-temperature degradation of Y-TZP.
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