Leelaphiwat Pattarin, Harte Janice B, Auras Rafael A, Ong Peter Kc, Chonhenchob Vanee
Department of Packaging and Materials Technology, Kasetsart University, Bangkok, 10900, Thailand.
Department of Food Science and Human Nutrition, Michigan State University, East Lansing, MI, 48824, USA.
J Sci Food Agric. 2017 Apr;97(6):1854-1860. doi: 10.1002/jsfa.7986. Epub 2016 Sep 5.
Changes in the aroma characteristics of Thai 'tom yam' seasoning powder, containing lemongrass, galangal and kaffir lime leaf, as affected by different packaging materials were assessed using quantitative descriptive analysis (QDA) and gas chromatography-mass spectrometry (GC-MS). The descriptive aroma attributes for lemongrass, galangal and kaffir lime leaf powders were developed by the QDA panel. The mixed herb and spice seasoning powder was kept in glass jars closed with different packaging materials (Nylon 6, polyethylene terephthalate (PET) and polylactic acid (PLA)) stored at 38 °C (accelerated storage condition), and evaluated by the trained QDA panel during storage for 49 days.
The descriptive words for Thai 'tom yam' seasoning powder developed by the trained panelists were lemongrass, vinegary and leafy for lemongrass, galangal and kaffir lime leaf dried powder, respectively. The aroma intensities significantly (P ≤ 0.05) decreased with increased storage time. However, the intensity scores for aroma attributes were not significantly (P > 0.05) different among the packaging materials studied. The major components in Thai 'tom yam' seasoning powder, quantified by GC-MS, were estragole, bicyclo[3.1.1]heptane, β-bisabolene, benzoic acid and 2-ethylhexyl salicylate. The concentrations of major aroma compounds significantly (P ≤ 0.05) decreased with storage time.
Aroma stability of Thai 'tom yam' powder can be determined by descriptive sensory evaluation and GC-MS analysis. Nylon, PET and PLA exhibited similar aroma barrier properties against key aroma compounds in Thai 'tom yam'. This information can be used for prediction of aroma loss through packaging materials during storage of Thai 'tom yam'. © 2016 Society of Chemical Industry.
采用定量描述分析(QDA)和气相色谱 - 质谱联用(GC - MS)技术,评估了含柠檬草、高良姜和青柠叶的泰国“冬阴功”调味粉在不同包装材料影响下的香气特征变化。QDA小组确定了柠檬草、高良姜和青柠叶粉末的描述性香气属性。将混合草本香料调味粉置于用不同包装材料(尼龙6、聚对苯二甲酸乙二酯(PET)和聚乳酸(PLA))密封的玻璃罐中,在38°C(加速储存条件)下储存,并由经过培训的QDA小组在49天的储存期内进行评估。
经过培训的小组成员确定的泰国“冬阴功”调味粉的描述性词汇分别为,柠檬草粉末的柠檬草味、醋味和叶味,高良姜粉末的高良姜味,以及青柠叶粉末的叶味。香气强度随储存时间延长而显著(P≤0.05)降低。然而,在所研究的包装材料中,香气属性的强度得分并无显著(P>0.05)差异。通过GC - MS定量分析得出,泰国“冬阴功”调味粉中的主要成分是草蒿脑、双环[3.1.1]庚烷、β - 红没药药烯烯、苯甲酸和2 - 乙基己基水杨酸酯。主要香气化合物的浓度随储存时间显著(P≤0.05)降低。
泰国“冬阴功”粉末的香气稳定性可通过描述性感官评价和GC - MS分析来确定。尼龙、PET和PLA对泰国“冬阴功”中的关键香气化合物表现出相似的香气阻隔性能。这些信息可用于预测泰国“冬阴功”在储存过程中通过包装材料造成的香气损失。©2016化学工业协会