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通过固相萃取和带火焰热离子检测的气相色谱法对血清中敌百虫进行快速灵敏的定量分析。

A rapid and sensitive quantitation of Dipterex in serum by solid-phase extraction and gas chromatography with flame thermionic detection.

作者信息

Ameno K, Fuke C, Ameno S, Kiriu T, Ijiri I

机构信息

Department of Forensic Medicine, Kagawa Medical School, Japan.

出版信息

J Anal Toxicol. 1989 May-Jun;13(3):150-1. doi: 10.1093/jat/13.3.150.

DOI:10.1093/jat/13.3.150
PMID:2755086
Abstract

A simple, sensitive, and rapid quantitative method for Dipterex in serum is described. A SepPak C18 cartridge for the extraction and gas chromatography with flame thermionic detection for determination are used. The detection limit is 2.5 ng/mL, and linearity is obtained in the range 5-500 ng/mL.

摘要

本文描述了一种用于测定血清中敌百虫的简单、灵敏且快速的定量方法。采用SepPak C18柱进行萃取,并使用火焰热离子检测气相色谱法进行测定。检测限为2.5 ng/mL,在5 - 500 ng/mL范围内呈线性。

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