塞尔维亚市场上罐装金枪鱼和沙丁鱼中的有机氯农药
Organochlorine pesticides in canned tuna and sardines on the Serbian market.
作者信息
Kartalović Brankica, Novakov Nikolina J, Mihaljev Željko, Petrović Jelena, Prica Nadežda, Babić Jelena, Ćirković Miroslav A
机构信息
a Department for food and feed quality, Bureau for food safety and drug analysis , Scientific veterinary institute Novi Sad , Novi Sad , Serbia.
b Department of Veterinary Medicine , University of Novi Sad , Novi Sad , Serbia.
出版信息
Food Addit Contam Part B Surveill. 2016 Dec;9(4):299-304. doi: 10.1080/19393210.2016.1234004. Epub 2016 Sep 19.
The aim of this study was to determine the level of organochlorine (OC) pesticides in 57 samples of canned tuna and 31 samples of canned sardines in vegetable oil, collected from supermarkets in Serbia. OC pesticides α-HCH, β-HCH, δ-HCH, dichlorodiphenyltrichloroethane (DDT), DDE, DDD, dielderin, endosulfane I, endosulfane II, endosulan sulfate, endrin, endrin ketone, heptachlor, heptachlor epoxide, lindane, aldrin, metoxichlor, cis-chlordane and trans-chlordane were determined using a GS-MS method. The highest concentrations (µg kg, arithmetic means) in canned tuna were for δ-HCH (60.6 ± 97.0) and p, p´-DDT (55.0 ± 25.1), while the corresponding values in canned sardines were for δ-HCH (90.7 ± 102.7) and endosulfane II (78.0 ± 145.9). Mean level for the sum of endosulfans was above the maximum limit in canned sardines (85.0 µg kg). Also, dieldrin (39.7 µg kg) was measured above the ML.
本研究的目的是测定从塞尔维亚超市采集的57份金枪鱼罐头样本和31份植物油沙丁鱼罐头样本中的有机氯（OC）农药含量。使用气相色谱-质谱联用（GS-MS）方法测定了OC农药α-六氯环己烷、β-六氯环己烷、δ-六氯环己烷、二氯二苯三氯乙烷（DDT）、滴滴伊、滴滴滴、狄氏剂、硫丹I、硫丹II、硫丹硫酸酯、异狄氏剂、异狄氏剂酮、七氯、七氯环氧化物、林丹、艾氏剂、甲氧滴滴涕、顺式氯丹和反式氯丹的含量。金枪鱼罐头中含量最高（μg/kg，算术平均值）的是δ-六氯环己烷（60.6±97.0）和p,p'-DDT（55.0±25.1），而植物油沙丁鱼罐头中的相应值是δ-六氯环己烷（90.7±102.7）和硫丹II（78.0±145.9）。植物油沙丁鱼罐头中硫丹总量的平均水平高于最大限量（85.0μg/kg）。此外，狄氏剂（39.7μg/kg）的测量值也高于最大限量。
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