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荜茇提取物中,Naviglio辅助提取法的优化及胡椒碱含量的测定。

Optimisation of a Naviglio-assisted extraction followed by determination of piperine content in Piper longum extracts.

作者信息

Gigliarelli Giulia, Pagiotti Rita, Persia Diana, Marcotullio Maria Carla

机构信息

a Department of Pharmaceutical Sciences , University of Perugia , Perugia , Italy.

出版信息

Nat Prod Res. 2017 Jan;31(2):214-217. doi: 10.1080/14786419.2016.1217209. Epub 2016 Aug 12.

Abstract

Studies were made to increase the yield of piperine extraction using Naviglio Extractor® solid-liquid dynamic extractor (SLDE) from fruits of Piper longum. The effects of ratio w/v were investigated and optimised for the best method. The maximum yield of piperine (317.7 mg/g) from P. longum fruits was obtained in SLDE 1:50 ethanol extract. Extraction yields of piperine obtained from Soxhlet extraction, decotion (International Organization for Standardization) and conventional maceration extraction methods were found to be 233.7, 231.8 and 143.6 mg/g, respectively. The results of the present study indicated that Naviglio Extractor® is an effective technique for the extraction of piperine from long pepper.

摘要

开展了多项研究,以提高使用纳维利奥萃取器®固液动态萃取器(SLDE)从荜茇果实中提取胡椒碱的产量。研究了料液比的影响,并对最佳方法进行了优化。在SLDE 1:50乙醇提取物中,荜茇果实中胡椒碱的最大产量为317.7毫克/克。索氏提取法、煎煮法(国际标准化组织)和传统浸渍提取法获得的胡椒碱提取率分别为233.7、231.8和143.6毫克/克。本研究结果表明,纳维利奥萃取器®是从荜茇中提取胡椒碱的有效技术。

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