Liu Lei, Yu Xiuzhu, Zhao Zhong, Xu Lirong, Zhang Rui
College of Food Science and Engineering, Northwest A&F University, Yangling, Shaanxi, China.
College of Forestry, Northwest A&F University, Yangling, Shaanxi, China.
J Sci Food Agric. 2017 Aug;97(11):3814-3821. doi: 10.1002/jsfa.8245. Epub 2017 Feb 27.
Salt-aided aqueous extraction (SAAE) is an inexpensive and environmentally friendly method of oil extraction that is influenced by many factors. In the present study, we investigated the effect of SAAE on bitter almond oil yield.
This study used sodium bicarbonate solution as extraction solvent and the optimal extraction parameters predicted by Box-Behnken design (i.e., concentration of sodium bicarbonate, 0.4 mol L ; solvent-to-sample ratio, 5:1; extraction temperature, 84 °C; extraction time, 60 min), for oil recovery of 90.9%. The physiochemical characteristics of the extracted oil suggest that the quality was similar to that of the aqueous enzymatic extracted oil. Moreover, the content of hydrocyanic acid (HCN) in bitter almond oil was found to be less than 5 mg kg , which was lower compared to that obtained by other reported methods. Results of microanalysis indicated that SAAE led to significant improvement in oil yield by allowing the release of oil and decreasing the emulsion fraction. Therefore, extraction of bitter almond oil by SAAE is feasible.
These results demonstrate that extraction of bitter almond oil by SAAE based on the salt effect is feasible on a laboratory scale. © 2017 Society of Chemical Industry.
盐辅助水相萃取(SAAE)是一种廉价且环保的油提取方法,受多种因素影响。在本研究中,我们研究了SAAE对苦杏仁油产量的影响。
本研究使用碳酸氢钠溶液作为萃取溶剂,并采用Box-Behnken设计预测的最佳萃取参数(即碳酸氢钠浓度为0.4 mol/L;溶剂与样品比例为5:1;萃取温度为84°C;萃取时间为60分钟),油回收率为90.9%。萃取油的理化特性表明其质量与水酶法萃取油相似。此外,发现苦杏仁油中氢氰酸(HCN)含量低于5 mg/kg,与其他报道方法相比更低。微观分析结果表明,SAAE通过促进油的释放和降低乳化率显著提高了油产量。因此,用SAAE萃取苦杏仁油是可行的。
这些结果表明,基于盐效应的SAAE法在实验室规模上萃取苦杏仁油是可行的。© 2017化学工业协会。