Quine Richard W, Rinard George A, Shi Yilin, Buchanan Laura, Biller Joshua R, Eaton Sandra S, Eaton Gareth R
Ritchie School of Engineering and Computer Science, University of Denver, Denver, Colorado 80210 USA.
Department of Chemistry and Biochemistry, University of Denver, Denver, Colorado, 80210 USA.
Concepts Magn Reson Part B Magn Reson Eng. 2016 Jul;46B(3):123-133. doi: 10.1002/cmr.b.21328.
A spectrometer was designed and constructed to facilitate measurements of T, T, spin echo signal-to-noise, and resonator quality factor, Q, between about 400 and 1000 MHz. Pulse patterns are generated at 250 MHz and mixed with the output from a second source to perform excitation and detection. A cross-loop resonator was constructed in which the same sample could be measured in the same resonator over the full range of frequencies. An air-core, 4-coil, water-cooled electromagnet with a large experimental volume was built.
设计并制造了一台光谱仪,以方便在约400至1000兆赫兹之间测量T、T、自旋回波信噪比和谐振器品质因数Q。在250兆赫兹下生成脉冲模式,并与第二个源的输出混合,以进行激发和检测。构建了一个交叉环谐振器,在该谐振器中,可以在整个频率范围内的同一谐振器中测量同一样品。制造了一个具有大实验体积的空心、4线圈、水冷电磁铁。