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基于硅酸三钙的根管倒充填材料的物理化学性质及牙本质粘结强度

Physicochemical Properties and Dentin Bond Strength of a Tricalcium Silicate-Based Retrograde Material.

作者信息

Lucas Camila de Paula Telles Pires, Viapiana Raqueli, Bosso-Martelo Roberta, Guerreiro-Tanomaru Juliane Maria, Camilleri Josette, Tanomaru-Filho Mário

机构信息

Department of Restorative Dentistry, Araraquara Dental School, UNESP - Universidade Estadual Paulista, Araraquara, SP, Brazil.

Department of Restorative Dentistry, Faculty of Dental Surgery, University of Malta, MaltaBrasil.

出版信息

Braz Dent J. 2017 Jan-Feb;28(1):51-56. doi: 10.1590/0103-6440201701135.

DOI:10.1590/0103-6440201701135
PMID:28301018
Abstract

The aim of this study was to evaluate the physicochemical properties and the apical dentin bond strength of the tricalcium silicate-based Biodentine in comparison to white MTA and zinc oxide eugenol-based cement (ZOE). Setting time and radiopacity were evaluated according to ISO 6876:2012 specification. Final setting time, compressive strength and pH were also assessed. Material's bond strength to the apical root canal dentin was measured by the push-out assay. Data were analyzed by ANOVA and Tukey-Krammer post-hoc test. Biodentine presented the shortest initial (16.2±1.48 min) and final setting time (35.4±5.55 min). Radiopacity of Biodentine (2.79±0.27 mmAl) does not agree with ISO 6876:2012 specifications. On the other hand, Biodentine showed higher compressive strength after 21 days (37.22±5.27 MPa) and higher dentin bond strength (11.2±2.16 MPa) in comparison to white MTA (27.68±3.56 MPa for compressive strength and 2.98±0.64 MPa for bond strength) (p<0.05). Both MTA and Biodentine produced an alkaline environment (approximately pH 10) (p>0.05) compared to ZOE (pH 7). It may be concluded that Biodentine exhibited faster setting, higher long-term compressive strength and bond strength to the apical dentin than MTA and ZOE.

摘要

本研究的目的是评估硅酸三钙基生物陶瓷(Biodentine)与白色矿物三氧化物聚合体(MTA)和氧化锌丁香酚基水门汀(ZOE)相比的物理化学性质和根尖牙本质粘结强度。根据ISO 6876:2012规范评估凝固时间和射线不透性。还评估了最终凝固时间、抗压强度和pH值。通过推出试验测量材料与根尖根管牙本质的粘结强度。数据采用方差分析和Tukey-Krammer事后检验进行分析。生物陶瓷(Biodentine)的初始凝固时间最短(16.2±1.48分钟),最终凝固时间也最短(35.4±5.55分钟)。生物陶瓷(Biodentine)的射线不透性(2.79±0.27 mmAl)不符合ISO 6876:2012规范。另一方面,与白色MTA相比,生物陶瓷(Biodentine)在21天后显示出更高的抗压强度(37.22±5.27 MPa)和更高的牙本质粘结强度(11.2±2.16 MPa)(白色MTA的抗压强度为27.68±3.56 MPa,粘结强度为2.98±0.64 MPa)(p<0.05)。与ZOE(pH值7)相比,MTA和生物陶瓷(Biodentine)均产生碱性环境(约pH值10)(p>0.05)。可以得出结论,与MTA和ZOE相比,生物陶瓷(Biodentine)凝固更快,对根尖牙本质的长期抗压强度和粘结强度更高。

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