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经空气喷砂处理的传统型和高透明度Y-TZP牙科陶瓷的特性研究

Characterization of Conventional and High-Translucency Y-TZP Dental Ceramics Submitted to Air Abrasion.

作者信息

Tostes Bhenya Ottoni, Guimarães Renato Bastos, Noronha-Filho Jaime Dutra, Botelho Glauco Dos Santos, Guimarães José Guilherme Antunes, Silva Eduardo Moreira da

机构信息

Analytical Laboratory of Restorative Biomaterials - LABiom-R, Dental School, UFF - Universidade Federal Fluminense, Niterói, RJ, Brazil.

Physics Institute, UFF - Universidade Federal Fluminense, Niterói, RJ, Brazil.

出版信息

Braz Dent J. 2017 Jan-Feb;28(1):97-104. doi: 10.1590/0103-6440201701035.

Abstract

This study evaluated the effect of air-abrasion on t®m phase transformation, roughness, topography and the elemental composition of three Y-TZP (Yttria-stabilized tetragonal zirconia polycrystal) dental ceramics: two conventional (Lava Frame and IPS ZirCad) and one with high-translucency (Lava Plus). Plates obtained from sintered blocks of each ceramic were divided into four groups: AS (as-sintered); 30 (air-abrasion with 30 mm Si-coated Al2O3 particles); 50 (air-abrasion with 50 mm Al2O3 particles) and 150 (air-abrasion with 150 mm Al2O3 particles). After the treatments, the plates were submitted to X-ray diffractometry; 3-D profilometry and SEM/EDS. The AS surfaces were composed of Zr and t phases. All treatments produced t®m phase transformation in the ceramics. The diameter of air-abrasion particles influenced the roughness (150>50>30>AS) and the topography. SEM analysis showed that the three treatments produced groove-shaped microretentions on the ceramic surfaces, which increased with the diameter of air-abrasion particles. EDS showed a decrease in Zr content along with the emergence of O and Al elements after air-abrasion. Presence of Si was also detected on the plates air-abraded with 30 mm Si-coated Al2O3 particles. It was concluded that irrespective of the type and diameter of the particles, air-abrasion produced t®m phase transformation, increased the roughness and changed the elemental composition of the three Y-TZP dental ceramics. Lava Plus also behaved similarly to the conventional Y-TZP ceramics, indicating that this high translucency ceramic could be more suitable to build monolithic ceramic restorations in the aesthetic restorative dentistry field.

摘要

本研究评估了空气喷砂对三种钇稳定四方多晶氧化锆(Y-TZP)牙科陶瓷的t®m相变、粗糙度、表面形貌和元素组成的影响:两种传统陶瓷(Lava Frame和IPS ZirCad)以及一种高透明度陶瓷(Lava Plus)。从每种陶瓷的烧结块上获得的板材被分为四组:AS(烧结态);30(用30μm硅涂层Al2O3颗粒进行空气喷砂);50(用50μm Al2O3颗粒进行空气喷砂)和150(用150μm Al2O3颗粒进行空气喷砂)。处理后,对板材进行X射线衍射分析、三维轮廓测量和扫描电子显微镜/能谱分析(SEM/EDS)。AS表面由Zr和t相组成。所有处理均使陶瓷发生t®m相变。空气喷砂颗粒的直径影响粗糙度(150>50>30>AS)和表面形貌。扫描电子显微镜分析表明,三种处理均在陶瓷表面产生了沟槽状微固位形,且随着空气喷砂颗粒直径的增大而增加。能谱分析表明,空气喷砂后Zr含量降低,同时出现了O和Al元素。在用30μm硅涂层Al2O3颗粒进行空气喷砂的板材上也检测到了Si的存在。研究得出结论,无论颗粒的类型和直径如何,空气喷砂都会使三种Y-TZP牙科陶瓷发生t®m相变、增加粗糙度并改变其元素组成。Lava Plus的表现也与传统Y-TZP陶瓷相似,这表明这种高透明度陶瓷可能更适合在美学修复牙科领域制作整体陶瓷修复体。

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