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新型飞秒激光对高透明氧化锆进行图案化处理作为传统颗粒研磨的替代方法

Novel Femto Laser Patterning of High Translucent Zirconia as an Alternative to Conventional Particle Abrasion.

作者信息

Tzanakakis Emmanouil-George C, Beketova Anastasia, Papadopoulou Lambrini, Kontonasaki Eleana, Tzoutzas Ioannis G

机构信息

School of Dentistry, National and Kapodistrian University of Athens, 2 Thivon Str, Goudi, 11527 Athens, Greece.

Department of Prosthodontics, School of Dentistry, Faculty of Health Sciences, Aristotle University of Thessaloniki, 54124 Thessaloniki, Greece.

出版信息

Dent J (Basel). 2021 Feb 8;9(2):20. doi: 10.3390/dj9020020.

Abstract

BACKGROUND

currently applied surface treatments for zirconia bonding may create undesired microcracks and surface flaws. The aim of the present study was to evaluate the efficacy of alternative surface treatments on the shear bond strength of high translucency zirconia to 10-Methacryloyloxydecyl dihydrogen phosphate (MDP)-containing resin-based cement.

METHODS

fifty disk-shaped specimens (10 mm × 5 mm) were fabricated from a commercial yttria-stabilized zirconia with 5 mole% yttrium oxide tetragonal zirconia polycrystal (5Y-TZP), and underwent air-abrasion with alumina particles (50 μm-AL50 and 90 μm-AL90), glass beads (GB 10-60 μm), and ablation with femtosecond laser (FEMTO). Shear bond strength was evaluated with a universal testing machine under a crosshead speed of 0.5 mm/min until fracture. Fracture type was evaluated with an optical stereomicroscope. Differences among groups were evaluated by one-way ANOVA and Bonferroni pairwise comparison tests ( < 0.05).

RESULTS

the highest shear bond strength values were presented by the laser treated group (23.97 ± 3.7 MPa). No statistically significant differences were found among the Cl, Al50, Al90 and FEMTO groups. The lowest mean value was presented by the glass-beads treated group (11.93 ± 2.88 MPa) which was significantly lower compared to all other groups ( < 0.001).

CONCLUSIONS

under the limitations of this in vitro study, femtosecond laser treatment of High-translucent monolithic zirconia (HTZ) ceramics is a promising alternative method for the mechanical retention of resin cements.

摘要

背景

目前用于氧化锆粘结的表面处理可能会产生不良的微裂纹和表面缺陷。本研究的目的是评估替代表面处理对高透明度氧化锆与含10 - 甲基丙烯酰氧基癸基二氢磷酸酯(MDP)的树脂基水门汀之间剪切粘结强度的效果。

方法

用含有5摩尔%氧化钇的四方氧化锆多晶体(5Y-TZP)的商用氧化钇稳定氧化锆制作50个圆盘形试样(10毫米×5毫米),并用氧化铝颗粒(50μm-AL50和90μm-AL90)、玻璃珠(GB 10 - 60μm)进行空气研磨,并用飞秒激光(FEMTO)进行烧蚀。使用万能试验机在0.5毫米/分钟的十字头速度下评估剪切粘结强度,直至断裂。用光学立体显微镜评估断裂类型。通过单因素方差分析和Bonferroni两两比较检验评估组间差异(<0.05)。

结果

激光处理组呈现出最高的剪切粘结强度值(23.97±3.7兆帕)。在Cl、Al50、Al90和FEMTO组之间未发现统计学上的显著差异。玻璃珠处理组呈现出最低的平均值(11.93±2.88兆帕),与所有其他组相比显著更低(<0.001)。

结论

在本体外研究的局限性下,飞秒激光处理高透明度整体式氧化锆(HTZ)陶瓷是一种有前景的用于树脂水门汀机械固位的替代方法。

https://cdn.ncbi.nlm.nih.gov/pmc/blobs/c4e4/7915195/254f06747e4f/dentistry-09-00020-g001.jpg

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