Lan Fei, Jiang Minlin, Tao Quan, Wei Fanan, Li Guangyong
Department of Electrical and Computer Engineering, University of Pittsburgh, Pittsburgh, Pennsylvania 15261, USA.
School of Machine Engineering and Automation, Fuzhou University, Fujian 350116, China.
Rev Sci Instrum. 2017 Mar;88(3):033704. doi: 10.1063/1.4978282.
A Kelvin probe force microscopy (KPFM) image is sometimes difficult to interpret because it is a blurred representation of the true surface potential (SP) distribution of the materials under test. The reason for the blurring is that KPFM relies on the detection of electrostatic force, which is a long-range force compared to other surface forces. Usually, KPFM imaging model is described as the convolution of the true SP distribution of the sample with an intrinsic point spread function (PSF) of the measurement system. To restore the true SP signals from the blurred ones, the intrinsic PSF of the system is needed. In this work, we present a way to experimentally calibrate the PSF of the KPFM system. Taking the actual probe shape and experimental parameters into consideration, this calibration method leads to a more accurate PSF than the ones obtained from simulations. Moreover, a nonlinear reconstruction algorithm based on total variation (TV) regularization is applied to KPFM measurement to reverse the blurring caused by PSF during KPFM imaging process; as a result, noises are reduced and the fidelity of SP signals is improved.
开尔文探针力显微镜(KPFM)图像有时难以解读,因为它是被测材料真实表面电势(SP)分布的模糊呈现。造成模糊的原因是KPFM依赖于静电力的检测,与其他表面力相比,静电力是一种长程力。通常,KPFM成像模型被描述为样品真实SP分布与测量系统固有点扩散函数(PSF)的卷积。为了从模糊信号中恢复真实的SP信号,需要系统的固有PSF。在这项工作中,我们提出了一种通过实验校准KPFM系统PSF的方法。考虑到实际探针形状和实验参数,这种校准方法得到的PSF比模拟得到的更准确。此外,一种基于总变分(TV)正则化的非线性重建算法被应用于KPFM测量,以消除KPFM成像过程中由PSF引起的模糊;结果,噪声减少,SP信号的保真度得到提高。