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不同遮光剂对实验性牙科复合树脂透明度的影响。

The effects of different opacifiers on the translucency of experimental dental composite resins.

作者信息

Haas Karine, Azhar Gulelala, Wood Duncan J, Moharamzadeh Keyvan, van Noort Richard

机构信息

School of Clinical Dentistry, University of Sheffield, Claremont Crescent, Sheffield S10 2TA, United Kingdom.

School of Clinical Dentistry, University of Sheffield, Claremont Crescent, Sheffield S10 2TA, United Kingdom.

出版信息

Dent Mater. 2017 Aug;33(8):e310-e316. doi: 10.1016/j.dental.2017.04.026. Epub 2017 May 20.

Abstract

OBJECTIVE

The aim of this study was to evaluate the effects of different opacifiers on the translucency of experimental dental composite-resins.

METHODS

Three metal oxides that are used as opacifiers were tested in this study: titanium oxide (TiO), aluminium oxide (AlO) and zirconium oxide (ZrO). Experimental composite-resins were fabricated containing 25wt.% urethane dimethacrylate (UDMA)-based resin matrix and 75% total filler including different concentrations of metal oxides (0, 0.25, 0.5, 0.75 and 1wt.%) blended into silane treated barium-silicate filler. The specimens (15.5mm diameter and 1mm thickness) were light-cured and tested in the transmittance mode using a UV/VIS spectrophotometer at wavelengths from 380 to 700nm under a standard illuminant D65. The color differences (ΔE* ab) between different concentrations of opacifiers were also measured in transmittance mode based on their Lab values.

RESULTS

Statistical analysis by ANOVA and Tukey's test showed a significant decrease (p<0.05) in light transmittance with the addition of opacifiers to the experimental composite-resins. There was a linear correlation between different concentrations of TiO and AlO and total transmittance. Total transmittance was also found to be wavelength dependent. The color differences for the concentrations of 0-1wt.% of the opacifiers were above 1 ΔE* unit, with AlO showing the smallest color shift.

SIGNIFICANCE

The type and the amount of the opacifiers used in this study had a significant effect on the translucency of the experimental UDMA-based dental composite resins. The most effective opacifier was TiO, followed by ZrO and AlO in decreasing order, respectively.

摘要

目的

本研究旨在评估不同遮光剂对实验性牙科复合树脂透明度的影响。

方法

本研究测试了三种用作遮光剂的金属氧化物:氧化钛(TiO)、氧化铝(AlO)和氧化锆(ZrO)。制备实验性复合树脂,其包含25wt.%的基于聚氨酯二甲基丙烯酸酯(UDMA)的树脂基质和75%的总填料,其中包括不同浓度(0、0.25、0.5、0.75和1wt.%)混入经硅烷处理的钡硅酸盐填料中的金属氧化物。将试样(直径15.5mm,厚度1mm)光固化,并在标准照明体D65下,使用紫外/可见分光光度计在380至700nm波长下以透射率模式进行测试。还基于不同浓度遮光剂的Lab值,在透射率模式下测量其颜色差异(ΔE* ab)。

结果

方差分析(ANOVA)和Tukey检验的统计分析表明,向实验性复合树脂中添加遮光剂后,透光率显著降低(p<0.05)。不同浓度的TiO和AlO与总透光率之间存在线性相关性。还发现总透光率与波长有关。遮光剂浓度为0 - 1wt.%时的颜色差异大于1个ΔE*单位,其中AlO的颜色变化最小。

意义

本研究中使用的遮光剂的类型和用量对基于UDMA的实验性牙科复合树脂的透明度有显著影响。最有效的遮光剂是TiO,其次是ZrO和AlO,依次递减。

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