Okada Masahiro, Inoue Kazusa, Irie Masao, Taketa Hiroaki, Torii Yasuhiro, Matsumoto Takuya
Department of Biomaterials, Graduate School of Medicine, Dentistry and Pharmaceutical Sciences, Okayama University.
Department of Comprehensive Dentistry, Okayama University Hospital.
Dent Mater J. 2017 Sep 26;36(5):600-605. doi: 10.4012/dmj.2016-334. Epub 2017 May 30.
Resin bonding to zirconia ceramics is difficult to achieve using the standard methods for conventional silica-based dental ceramics, which employ silane coupling monomers as primers. The hypothesis in this study was that a silane coupling oligomer -a condensed product of silane coupling monomers- would be a more suitable primer for zirconia. To prove this hypothesis, the shear bond strengths between a composite resin and zirconia were compared after applying either a silane coupling monomer or oligomer. The shear bond strength increased after applying a non-activated ethanol solution of the silane coupling oligomer compared with that achieved when applying the monomer. Thermal treatment of the zirconia at 110°C after application of the silane coupling agents was essential to improve the shear bond strength between the composite resin cement and zirconia.
使用传统的基于二氧化硅的牙科陶瓷的标准方法来实现树脂与氧化锆陶瓷的粘结很困难,传统方法使用硅烷偶联单体作为底漆。本研究的假设是,硅烷偶联低聚物——硅烷偶联单体的缩合产物——将是一种更适合氧化锆的底漆。为了验证这一假设,在应用硅烷偶联单体或低聚物后,比较了复合树脂与氧化锆之间的剪切粘结强度。与应用单体时相比,应用硅烷偶联低聚物的非活性乙醇溶液后,剪切粘结强度有所提高。在应用硅烷偶联剂后,将氧化锆在110°C下进行热处理对于提高复合树脂粘结剂与氧化锆之间的剪切粘结强度至关重要。