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制备并表征了包埋表没食子儿茶素没食子酸酯纳米胶囊的抗氧化可食用壳聚糖膜。

Preparation and characterization of antioxidant edible chitosan films incorporated with epigallocatechin gallate nanocapsules.

机构信息

State Key Laboratory of Tea Plant Biology and Utilization, Anhui Agricultural University, Hefei, China; Anhui Agricultural Products Processing Engineering Laboratory, Anhui Agricultural University, Hefei, China.

State Key Laboratory of Tea Plant Biology and Utilization, Anhui Agricultural University, Hefei, China.

出版信息

Carbohydr Polym. 2017 Sep 1;171:300-306. doi: 10.1016/j.carbpol.2017.04.081. Epub 2017 Apr 27.

Abstract

Antioxidant edible films based on chitosan hydrochloride (CHC) and epigallocatechin gallate (EGCG)-loaded nanocapsules (NCs) were developed. The CHC films incorporated with NCs were prepared by a casting method in three different proportions. The obtained films were characterized using the techniques including scanning electron microscopy, Fourier transform infrared spectroscopy and X-ray diffraction. Meanwhile, the mechanical and color properties, optical transmittance, EGCG release profile and antioxidant activity were also determined. The addition of NCs to CHC films increased their tensile strength (TS) and the percent elongation at break (%E). Lightness was significantly decreased in the NCs embedded films compared to controls, which in turn led to high antioxidant activity and excellent barrier properties against visible light. EGCG was rapidly released into food simulant although the concentration fluctuates over time. Therefore, these films can prevent the oxidation of fatty food stuffs.

摘要

基于壳聚糖盐酸盐(CHC)和表没食子儿茶素没食子酸酯(EGCG)负载纳米胶囊(NCs)的抗氧化可食用薄膜被开发出来。通过浇铸法,将 CHC 薄膜以三种不同的比例与 NCs 复合。采用扫描电子显微镜、傅里叶变换红外光谱和 X 射线衍射等技术对所得薄膜进行了表征。同时,还测定了薄膜的机械和颜色性能、透光率、EGCG 释放曲线和抗氧化活性。与对照相比,NCs 的加入提高了 CHC 薄膜的拉伸强度(TS)和断裂伸长率(%E)。嵌入 NCs 的薄膜的明度显著降低,这反过来又导致了高抗氧化活性和对可见光的优异阻隔性能。EGCG 虽然会随时间波动,但会迅速释放到食品模拟物中。因此,这些薄膜可以防止脂肪类食物的氧化。

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