Department of Food Science and Technology, National Nutrition and Food Technology Research Institute, Faculty of Nutrition Sciences and Food Technology, Shahid Beheshti University of Medical Sciences, Tehran, Iran.
Department of Physics, Shahid Beheshti University, Iran and Laser-Plasma Research Institute, Shahid Beheshti University, Tehran, Iran.
Int J Biol Macromol. 2017 Dec;105(Pt 1):121-130. doi: 10.1016/j.ijbiomac.2017.07.002. Epub 2017 Jul 4.
This study aimed to develop novel bilayer films based on alginate, chitosan and low-density polyethylene (LDPE) containing different concentrations of summer savory extract (SSE). The cold atmospheric plasma system was used to increase the surface energy of LDPE. Initially, water contact angle, surface roughness and the functional group of LDPE before and after plasma treatment were investigated. Then physical, mechanical, optical, antioxidant and microstructure properties of plasma-treated and untreated bilayer films and antioxidant films incorporated with SSE were characterized. Results showed that plasma treatment increased oxygen-containing the polar group, surface roughness and decreased water contact angle of LDPE surface (from 90.47° to 48.73°) and in result enhanced adhesion between polysaccharide coating and LDPE. Tensile strength of both alginate and chitosan coated-LDPE increased from 10.096 to 14.372 and 11.513 to 13.459MPa, respectively after plasma pretreatment. However chitosan-based films had lower water solubility. Although, incorporation of SSE into chitosan and alginate coated-LDPE despite slight adverse effects on the physical and mechanical properties of films, it provided antioxidant activity. Chitosan coated-LDPE containing SSE had potential to use as antioxidant food packaging.
本研究旨在开发基于海藻酸钠、壳聚糖和低密度聚乙烯(LDPE)的新型双层膜,其中含有不同浓度的荆芥提取物(SSE)。冷等离子体系统用于提高 LDPE 的表面能。首先,研究了等离子体处理前后 LDPE 的水接触角、表面粗糙度和官能团。然后,对等离子体处理和未处理的双层膜以及含有 SSE 的抗氧化膜的物理、机械、光学、抗氧化和微观结构性能进行了表征。结果表明,等离子体处理增加了 LDPE 表面的含氧极性基团,提高了表面粗糙度,降低了水接触角(从 90.47°降至 48.73°),从而增强了多糖涂层与 LDPE 的附着力。经等离子体预处理后,海藻酸钠和壳聚糖涂覆的 LDPE 的拉伸强度分别从 10.096 增至 14.372 和 11.513 增至 13.459MPa。然而,壳聚糖基膜的水溶性较低。尽管 SSE 掺入壳聚糖和海藻酸钠涂覆的 LDPE 会对膜的物理和机械性能产生轻微的不利影响,但它提供了抗氧化活性。含有 SSE 的壳聚糖涂覆的 LDPE 具有作为抗氧化食品包装的潜力。