Liebermann Anja, Roos Malgorzata, Stawarczyk Bogna
Department of Prosthodontics, Dental School, Ludwig-Maximilians-University Munich, Goethestrasse 70, 80336 Munich, Germany.
Department of Biostatistics at Epidemiology, Biostatistics and Prevention Institute, University of Zurich, Hirschgraben 84, 8001 Zurich, Switzerland.
Materials (Basel). 2017 Mar 16;10(3):300. doi: 10.3390/ma10030300.
The aim of this study was to analyze the long-term color stability of eight self-adhesive composite resin cements (SACRCs) after storage in diverse media for up to one year. 480 discs (diameter: 12 mm/thickness: 1.0 ± 0.05 mm) were fabricated (n = 60/SACRC): (1) BeautyCem (BEA); (2) Bifix SE (BIF); (3) Clearfil SA Cement Automix (CLE); (4) RelyX Unicem 2 Automix (RXU); (5) SeT (SET); (6) SmartCem 2 (SMC); (7) SoloCem (SOC); and (8) SpeedCEM (SPC). After polishing, specimens were immersed in (a) red wine (RW); (b) curry-solution (CU); (c) cress-solution (CR); and (d) distilled water (DW) at 37 °C and measured after 7, 28, 90, 180, and 365 days for color differences (ΔE) and water absorption (WA). Non-aged specimens were used as baselines. After 365 days, all of the discs were polished and their ΔE was measured. Data were analyzed using Kolmogorov-Smirnov, partial-eta-squared/η², 3-/1-way ANOVA with Tukey-HSD post-hoc test (α = 0.05). Significant differences occurred between all SACRCs for WA ( ≤ 0.003), except in RXU and in SET and in ΔE ( ≤ 0.002), except in SET and SPC. The significantly highest WA presented in SOC; the lowest showed in BEA. Significant ΔE differences and a decrease after polishing between all storage media were found ( < 0.001) with highest values for RW, followed by CU, CR, and DW. The lowest ΔE was measured for CLE, followed by SOC, BIF, RXU, BEA, SPC, SET, and SMC ( < 0.001) and increased significantly during aging. The highest ΔE decrease presented in BEA. SACRCs showed an increase in WA/ΔE within total aging time. Discoloration could not be removed completely by polishing. SACRCs need to be carefully selected for restorations in the esthetical zone with visible restoration margins. Polishing can significantly reduce the marginal discoloration.
本研究旨在分析八种自粘复合树脂水门汀(SACRCs)在不同介质中储存长达一年后的长期颜色稳定性。制备了480个圆盘(直径:12 mm/厚度:1.0±0.05 mm)(每种SACRCs n = 60):(1)BeautyCem(BEA);(2)Bifix SE(BIF);(3)Clearfil SA Cement Automix(CLE);(4)RelyX Unicem 2 Automix(RXU);(5)SeT(SET);(6)SmartCem 2(SMC);(7)SoloCem(SOC);和(8)SpeedCEM(SPC)。抛光后,将试样浸入(a)红酒(RW);(b)咖喱溶液(CU);(c)水芹溶液(CR);和(d)37℃的蒸馏水中(DW),并在7、28、90、180和365天后测量颜色差异(ΔE)和吸水率(WA)。未老化的试样用作基线。365天后,对所有圆盘进行抛光并测量其ΔE。使用Kolmogorov-Smirnov、偏η²、三因素/单因素方差分析和Tukey-HSD事后检验(α = 0.05)对数据进行分析。除RXU、SET以及ΔE(≤0.002)中的SET和SPC外,所有SACRCs的WA(≤0.003)之间均存在显著差异。SOC的WA显著最高;BEA的WA最低。在所有储存介质之间发现了显著的ΔE差异以及抛光后的降低(<0.001),RW的值最高,其次是CU、CR和DW。CLE的ΔE最低,其次是SOC、BIF、RXU、BEA、SPC、SET和SMC(<0.001),并且在老化过程中显著增加。BEA的ΔE降低最高。SACRCs在总老化时间内WA/ΔE增加。变色不能通过抛光完全去除。对于美学区域中修复边缘可见的修复体,需要仔细选择SACRCs。抛光可以显著减少边缘变色。