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航天部件增材制造中的挑战:粉末原料交叉污染及其对最终产品的影响。

Challenges in Additive Manufacturing of Space Parts: Powder Feedstock Cross-Contamination and Its Impact on End Products.

作者信息

Brandão Ana D, Gerard Romain, Gumpinger Johannes, Beretta Stefano, Makaya Advenit, Pambaguian Laurent, Ghidini Tommaso

机构信息

ESTEC, European Space Agency, 2200 AG Noordwijk, The Netherlands.

Politecnico di Milano, Via La Masa 1, 20156 Milan, Italy.

出版信息

Materials (Basel). 2017 May 12;10(5):522. doi: 10.3390/ma10050522.

Abstract

This work studies the tensile properties of Ti-6Al-4V samples produced by laser powder bed based Additive Manufacturing (AM), for different build orientations. The results showed high scattering of the yield and tensile strength and low fracture elongation. The subsequent fractographic investigation revealed the presence of tungsten particles on the fracture surface. Hence, its detection and impact on tensile properties of AM Ti-6Al-4V were investigated. X-ray Computed Tomography (X-ray CT) scanning indicated that these inclusions were evenly distributed throughout the samples, however the inclusions area was shown to be larger in the load-bearing plane for the vertical specimens. A microstructural study proved that the mostly spherical tungsten particles were embedded in the fully martensitic Ti-6Al-4V AM material. The particle size distribution, the flowability and the morphology of the powder feedstock were investigated and appeared to be in line with observations from other studies. X-ray CT scanning of the powder however made the high density particles visible, where various techniques, commonly used in the certification of powder feedstock, failed to detect the contaminant. As the detection of cross contamination in the powder feedstock proves to be challenging, the use of only one type of powder per AM equipment is recommended for critical applications such as Space parts.

摘要

这项工作研究了通过基于激光粉末床的增材制造(AM)生产的不同构建方向的Ti-6Al-4V样品的拉伸性能。结果表明,屈服强度和抗拉强度的分散性很高,断裂伸长率很低。随后的断口分析显示,断口表面存在钨颗粒。因此,对其检测及其对增材制造Ti-6Al-4V拉伸性能的影响进行了研究。X射线计算机断层扫描(X射线CT)表明,这些夹杂物在整个样品中均匀分布,然而,垂直试样的承载平面中的夹杂物面积更大。微观结构研究证明,大部分球形钨颗粒嵌入完全马氏体组织的增材制造Ti-6Al-4V材料中。对粉末原料的粒度分布、流动性和形态进行了研究,结果似乎与其他研究的观察结果一致。然而,对粉末进行X射线CT扫描时,高密度颗粒可见,而粉末原料认证中常用的各种技术均未能检测到污染物。由于证明检测粉末原料中的交叉污染具有挑战性,对于诸如航天部件等关键应用,建议在每个增材制造设备中仅使用一种类型的粉末。

https://cdn.ncbi.nlm.nih.gov/pmc/blobs/d5c7/5459071/0510675028db/materials-10-00522-g001.jpg

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