Khalil Khalil Abdelrazek, Sherif El-Sayed M, Nabawy A M, Abdo Hany S, Marzouk Wagih W, Alharbi Hamad F
Mechanical Engineering Department, College of Engineering, King Saud University, Al-Riyadh 11421, Saudi Arabia.
Mechanical Design and Materials Department, Faculty of Energy Engineering, Aswan University, Aswan 002097, Egypt.
Materials (Basel). 2016 May 20;9(5):399. doi: 10.3390/ma9050399.
TiC nanofibers reinforced Al matrix composites were produced by High Frequency Induction Heat Sintering (HFIHS).The titanium carbide nanofibers with an average diameter of 90 nm are first prepared by electrospinning technique and high temperature calcination process. A composite solution containing polyacrylonitrile and titanium isopropoxide is first electrospun into the nanofibers, which are subsequently stabilized and then calcined to produce the desired TiC nanofibers. The X-ray diffraction pattern and transmission electron microscopy results show that the main phase of the as-synthesized nanofibers is titanium carbide. The TiC nanofibers is then mixed with the aluminum powders and introduced into high frequency induction heat sintering (HFIHS) to produce composites of TiC nanofibers reinforced aluminum matrix. The potential application of the TiC nanofibers reinforced aluminum matrix composites was systematically investigated. 99.5% relative density and around 85 HV (833 MPa) Vickers hardness of the Al reinforced with 5 wt % TiC nanofiber has been obtained. Furthermore, the sample of Al contains 5 wt % TiC, has the highest value of compression and yield strength of about 415 and 350 MPa, respectively. The ductility of the Al/5 wt % TiC showed increasing with increasing the TiC contents.
采用高频感应热烧结(HFIHS)制备了TiC纳米纤维增强铝基复合材料。首先通过静电纺丝技术和高温煅烧工艺制备了平均直径为90nm的碳化钛纳米纤维。首先将含有聚丙烯腈和异丙醇钛的复合溶液静电纺丝成纳米纤维,随后对其进行稳定化处理,然后煅烧以制备所需的TiC纳米纤维。X射线衍射图谱和透射电子显微镜结果表明,合成的纳米纤维的主要相是碳化钛。然后将TiC纳米纤维与铝粉混合,并引入高频感应热烧结(HFIHS)中,以制备TiC纳米纤维增强铝基复合材料。系统研究了TiC纳米纤维增强铝基复合材料的潜在应用。用5wt%TiC纳米纤维增强的Al获得了99.5%的相对密度和约85HV(833MPa)的维氏硬度。此外,含5wt%TiC的Al样品的压缩强度和屈服强度最高,分别约为415MPa和350MPa。Al/5wt%TiC的延展性随TiC含量的增加而增加。