Alam Mohammad Azad, Ya Hamdan H, Yusuf Mohammad, Sivraj Ramaneish, Mamat Othman B, Sapuan Salit M, Masood Faisal, Parveez Bisma, Sattar Mohsin
Mechanical Engineering Department, Universiti Teknologi PETRONAS, Seri Iskandar 32610, Malaysia.
Chemical Engineering Department, Universiti Teknologi PETRONAS, Seri Iskandar 32610, Malaysia.
Materials (Basel). 2021 Aug 20;14(16):4703. doi: 10.3390/ma14164703.
The tenacious thirst for fuel-saving and desirable physical and mechanical properties of the materials have compelled researchers to focus on a new generation of aluminum hybrid composites for automotive and aircraft applications. This work investigates the microhardness behavior and microstructural characterization of aluminum alloy (Al 7075)-titanium carbide (TiC)-graphite (Gr) hybrid composites. The hybrid composites were prepared via the powder metallurgy technique with the amounts of TiC (0, 3, 5, and 7 wt.%), reinforced to Al 7075 + 1 wt.% Gr. The microstructural characteristics were investigated by optical microscopy, scanning electron microscopy (SEM), X-ray diffraction (XRD) and energy dispersive X-ray spectroscopy (EDS) elemental mapping. A Box Behnken design (BBD) response surface methodology (RSM) approach was utilized for modeling and optimization of density and microhardness independent parameters and to develop an empirical model of density and microhardness in terms of process variables. Effects of independent parameters on the responses have been evaluated by analysis of variance (ANOVA). The density and microhardness of the Al 7075-TiC-Gr hybrid composites are found to be increased by increasing the weight percentage of TiC particles. The optimal conditions for obtaining the highest density and microhardness are estimated to be 6.79 wt.% TiC at temperature 626.13 °C and compaction pressure of 300 Mpa.
对材料节油性能以及理想物理和机械性能的强烈渴望,促使研究人员将重点放在用于汽车和飞机应用的新一代铝基混杂复合材料上。这项工作研究了铝合金(Al 7075)-碳化钛(TiC)-石墨(Gr)混杂复合材料的显微硬度行为和微观结构表征。通过粉末冶金技术制备混杂复合材料,其中TiC的含量为(0、3、5和7 wt.%),增强到Al 7075 + 1 wt.% Gr中。通过光学显微镜、扫描电子显微镜(SEM)、X射线衍射(XRD)和能量色散X射线光谱(EDS)元素映射研究微观结构特征。采用Box Behnken设计(BBD)响应面方法(RSM)对密度和显微硬度独立参数进行建模和优化,并根据工艺变量建立密度和显微硬度的经验模型。通过方差分析(ANOVA)评估独立参数对响应的影响。发现通过增加TiC颗粒的重量百分比,Al 7075-TiC-Gr混杂复合材料的密度和显微硬度会增加。获得最高密度和显微硬度的最佳条件估计为在温度626.13 °C和压实压力300 Mpa下TiC含量为6.79 wt.%。