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Tunability of Size and Magnetic Moment of Iron Oxide Nanoparticles Synthesized by Forced Hydrolysis.

作者信息

Sutens Ben, Swusten Tom, Zhong Kuo, Jochum Johanna K, Van Bael Margriet J, Van der Eycken Erik V, Brullot Ward, Bloemen Maarten, Verbiest Thierry

机构信息

Department of Chemistry, Laboratory for Molecular Electronics and Photonics, KU Leuven, Celestijnenlaan 200D, Box 2425, 3001 Leuven, Belgium.

Department of Physics and Astronomy, Laboratory of Solid State Physics and Magnetism, KU Leuven, Celestijnenlaan 200D, 3001 Leuven, Belgium.

出版信息

Materials (Basel). 2016 Jul 8;9(7):554. doi: 10.3390/ma9070554.


DOI:10.3390/ma9070554
PMID:28773675
原文链接:https://pmc.ncbi.nlm.nih.gov/articles/PMC5456920/
Abstract

To utilize iron oxide nanoparticles in biomedical applications, a sufficient magnetic moment is crucial. Since this magnetic moment is directly proportional to the size of the superparamagnetic nanoparticles, synthesis methods of superparamagnetic iron oxide nanoparticles with tunable size are desirable. However, most existing protocols are plagued by several drawbacks. Presented here is a one-pot synthesis method resulting in monodisperse superparamagnetic iron oxide nanoparticles with a controllable size and magnetic moment using cost-effective reagents. The obtained nanoparticles were thoroughly characterized by transmission electron microscopy (TEM), X-ray diffraction (XRD) and Fourier transform infrared (FT-IR) measurements. Furthermore, the influence of the size on the magnetic moment of the nanoparticles is analyzed by superconducting quantum interference device (SQUID) magnetometry. To emphasize the potential use in biomedical applications, magnetic heating experiments were performed.

摘要
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/8656/5456920/e4d6984e18a8/materials-09-00554-g006.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/8656/5456920/25299fce4a74/materials-09-00554-g001.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/8656/5456920/0fc971d6c85e/materials-09-00554-g002.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/8656/5456920/c224f503ad08/materials-09-00554-g003.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/8656/5456920/1a5b45582124/materials-09-00554-g004.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/8656/5456920/27a11429fd1c/materials-09-00554-g005.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/8656/5456920/e4d6984e18a8/materials-09-00554-g006.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/8656/5456920/25299fce4a74/materials-09-00554-g001.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/8656/5456920/0fc971d6c85e/materials-09-00554-g002.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/8656/5456920/c224f503ad08/materials-09-00554-g003.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/8656/5456920/1a5b45582124/materials-09-00554-g004.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/8656/5456920/27a11429fd1c/materials-09-00554-g005.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/8656/5456920/e4d6984e18a8/materials-09-00554-g006.jpg

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Tunability of Size and Magnetic Moment of Iron Oxide Nanoparticles Synthesized by Forced Hydrolysis.

Materials (Basel). 2016-7-8

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[3]
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[4]
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[5]
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[6]
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本文引用的文献

[1]
Synthesis and Characterization of Holmium-Doped Iron Oxide Nanoparticles.

Materials (Basel). 2014-2-12

[2]
Broadband nonreciprocal quadrupolarization-induced asymmetric transmission (Q-AT) in plasmonic nanoparticle aggregates.

Adv Mater. 2015-3-9

[3]
Heterobifunctional PEG ligands for bioconjugation reactions on iron oxide nanoparticles.

PLoS One. 2014-10-2

[4]
Compact optical switch based on 2D photonic crystal and magneto-optical cavity.

Opt Lett. 2013-4-1

[5]
Controlled antibody/(bio-) conjugation of inorganic nanoparticles for targeted delivery.

Adv Drug Deliv Rev. 2012-12-29

[6]
Improved functionalization of oleic acid-coated iron oxide nanoparticles for biomedical applications.

J Nanopart Res. 2012-9

[7]
Characterization of magnetization-induced second harmonic generation in iron oxide polymer nanocomposites.

Appl Opt. 2012-1-10

[8]
Magnetic-plasmonic nanoparticles for the life sciences: calculated optical properties of hybrid structures.

Nanomedicine. 2011-9-21

[9]
Thiol-ene click reaction as a general route to functional trialkoxysilanes for surface coating applications.

J Am Chem Soc. 2011-7-5

[10]
Preparation of Monodisperse Iron Oxide Nanoparticles via the Synthesis and Decomposition of Iron Fatty Acid Complexes.

Nanoscale Res Lett. 2009-7-30

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