Yao Quantong, Sun Jian, Fu Yuzhu, Tong Weiping, Zhang Hui
Key Laboratory of Electromagnetic Processing of Materials, Ministry of Education, Northeastern University, Shenyang 110819, Liaoning, China.
Department of Materials Science and Engineering, Hefei University of Technology, Hefei 230009, Anhui, China.
Materials (Basel). 2016 Dec 8;9(12):993. doi: 10.3390/ma9120993.
In this paper, a nanocrystalline surface layer without impurities was fabricated on Ti-6Al-4V alloy by means of surface mechanical attrition treatment (SMAT). The grain size in the nanocrystalline layer is about 10 nm and grain morphology displays a random crystallographic orientation distribution. Subsequently, the low-temperature boriding behaviors (at 600 °C) of the SMAT sample, including the phase composition, microstructure, micro-hardness, and brittleness, were investigated in comparison with those of coarse-grained sample borided at 1100 °C. The results showed that the boriding kinetics could be significantly enhanced by SMAT, resulting in the formation of a nano-structured boride layers on Ti-6Al-4V alloy at lower temperature. Compared to the coarse-grained boriding sample, the SMAT boriding sample exhibits a similar hardness value, but improved surface toughness. The satisfactory surface toughness may be attributed to the boriding treatment that was carried out at lower temperature.
本文通过表面机械研磨处理(SMAT)在Ti-6Al-4V合金上制备了无杂质的纳米晶表层。纳米晶层中的晶粒尺寸约为10nm,晶粒形态呈现随机的晶体取向分布。随后,与在1100℃进行硼化处理的粗晶样品相比,研究了SMAT样品在600℃下的低温硼化行为,包括相组成、微观结构、显微硬度和脆性。结果表明,SMAT可显著提高硼化动力学,从而在较低温度下在Ti-6Al-4V合金上形成纳米结构硼化物层。与粗晶硼化样品相比,SMAT硼化样品具有相似的硬度值,但表面韧性有所提高。令人满意的表面韧性可能归因于在较低温度下进行的硼化处理。