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用于测定环境样品中镉的液相微萃取方法。

Methods of liquid phase microextraction for the determination of cadmium in environmental samples.

作者信息

Pires Santos Analú, das Graças Andrade Korn Maria, Azevedo Lemos Valfredo

机构信息

Universidade Federal da Bahia, Departamento de Química Analítica, Campus Universitário de Ondina, Instituto de Química, Salvador, Bahia, 40170-280, Brazil.

Universidade Estadual do Sudoeste da Bahia, Laboratório de Química Analítica (LQA), Campus de Jequié, Jequié, Bahia, 45206-510, Brazil.

出版信息

Environ Monit Assess. 2017 Aug 9;189(9):444. doi: 10.1007/s10661-017-6151-8.

DOI:10.1007/s10661-017-6151-8
PMID:28795304
Abstract

Liquid phase microextraction (LPME) has been widely used in extraction and preconcentration systems as an excellent alternative to conventional liquid phase extraction. In this work, a critical review is presented on liquid phase microextraction techniques used in the determination of cadmium in environmental samples. LPME techniques are classified into three main groups: single-drop liquid phase microextraction (SDME), hollow fiber liquid phase microextraction (HF-LPME), and dispersive liquid-liquid microextraction (DLLME). Methods involving these liquid phase microextraction techniques are described, addressing advantages and disadvantages, samples, figures of merit, and trends.

摘要

液相微萃取(LPME)作为传统液相萃取的一种绝佳替代方法,已在萃取和预浓缩系统中得到广泛应用。本文对用于测定环境样品中镉的液相微萃取技术进行了批判性综述。LPME技术主要分为三大类:单滴液相微萃取(SDME)、中空纤维液相微萃取(HF-LPME)和分散液液微萃取(DLLME)。文中描述了涉及这些液相微萃取技术的方法,讨论了其优缺点、样品、性能指标及发展趋势。

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Methods of liquid phase microextraction for the determination of cadmium in environmental samples.用于测定环境样品中镉的液相微萃取方法。
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本文引用的文献

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Determination of cadmium and lead at sub-ppt level in soft drinks: An efficient combination between dispersive liquid-liquid microextraction and graphite furnace atomic absorption spectrometry.软饮料中亚皮克级镉和铅的测定:分散液液微萃取与石墨炉原子吸收光谱法的高效结合
Food Chem. 2017 Apr 15;221:907-912. doi: 10.1016/j.foodchem.2016.11.075. Epub 2016 Nov 19.
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Simultaneous Preconcentration of Copper and Cadmium by Dispersive Liquid-Liquid Microextraction Using N,N'-Bis (2-Hydroxy-5-Bromo-Benzyl)1,2 Diaminopropane and Their Determination by Flame Atomic Absorption Spectrometry.使用N,N'-双(2-羟基-5-溴苄基)1,2-二氨基丙烷通过分散液液微萃取同时预富集铜和镉及其火焰原子吸收光谱法测定
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Vortex-assisted surfactant-enhanced-emulsification liquid-liquid microextraction with solidification of floating organic droplet combined with flame atomic absorption spectrometry for the fast determination of cadmium in water samples.涡旋辅助表面活性剂增强乳化液液微萃取结合漂浮有机液滴固化与火焰原子吸收光谱法快速测定水样中的镉
Water Sci Technol. 2016;73(11):2781-8. doi: 10.2166/wst.2016.063.
4
Cadmium minimization in wheat: A critical review.小麦中镉含量的最小化:一项批判性综述。
Ecotoxicol Environ Saf. 2016 Aug;130:43-53. doi: 10.1016/j.ecoenv.2016.04.001. Epub 2016 Apr 8.
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Dispersive Liquid-Liquid Microextraction Using Low-Toxic Solvent for the Determination of Heavy Metals in Water Samples by Inductively Coupled Plasma-Mass Spectrometry.
J AOAC Int. 2016 Jan-Feb;99(1):260-6. doi: 10.5740/jaoacint.15-0061. Epub 2016 Jan 28.
6
Switchable polarity solvent for liquid phase microextraction of Cd(II) as pyrrolidinedithiocarbamate chelates from environmental samples.用于从环境样品中液相微萃取镉(II)吡咯烷二硫代氨基甲酸盐螯合物的可切换极性溶剂。
Anal Chim Acta. 2015 Jul 30;886:75-82. doi: 10.1016/j.aca.2015.06.021. Epub 2015 Jul 9.
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Trace determination of lead, chromium and cadmium in herbal medicines using ultrasound-assisted emulsification microextraction combined with graphite furnace atomic absorption spectrometry.超声辅助乳化微萃取结合石墨炉原子吸收光谱法测定草药中的铅、铬和镉
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Temperature-controlled ionic liquid-based ultrasound-assisted microextraction for preconcentration of trace quantity of cadmium and nickel by using organic ligand in artificial saliva extract of smokeless tobacco products.基于温控离子液体的超声辅助微萃取法,用于在无烟烟草制品的人工唾液提取物中利用有机配体对痕量镉和镍进行预富集。
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