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掺入氟磷灰石纳米生物陶瓷对玻璃离子水门汀抗压强度和生物活性的影响

Influence of Incorporating Fluoroapatite Nanobioceramic on the Compressive Strength and Bioactivity of Glass Ionomer Cement.

作者信息

M Khaghani, S Alizadeh, A Doostmohammadi

机构信息

Young Researchers and Elite Club, Najafabad Branch, Islamic Azad University, Najafabad, Iran.

Materials Department, Engineering faculty, Shahrekord University, Shahrekord, Iran.

出版信息

J Dent Biomater. 2016 Sep;3(3):276-283.

Abstract

STATEMENT OF PROBLEM

In order to increase the performance of glass ionomer cement, it is reinforced with metal powders, short fibers, bioceramics and other materials. Fluoroapatite (Ca(PO)F) is found in dental enamel and is usually used in dental materials due to its good chemical and physical properties.

OBJECTIVES

In this study, the effects of the addition of synthesized fluoroapatite nanoceramic on the compressive strength and bioactivity of glass ionomer cement were investigated.

MATERIALS AND METHODS

The synthesized fluoroapatite nanoceramic particles (~ 70 nm) were incorporated into as-prepared glass ionomer powder and were characterized using X-ray diffraction (XRD), Fourier transform infrared spectroscopy (FTIR) and scanning electron microscopy (SEM). Moreover, the compressive strength values of the modified glass ionomer cements with 0, 1, 3 and 5 wt% of fluoroapatite were evaluated.

RESULTS

Results showed that glass ionomer cement containing 3 wt% fluoroapatite nanoparticles exhibited the highest compressive strength (102.6 ± 4) compared to the other groups, including control group. Furthermore, FTIR and SEM investigations indicated that after soaking the glass ionomer cement- 3 wt% fluoroapatite composite in the simulated body fluid solution, the intensity of O-H, P-O and C-O absorption bands increased as a result of the formation of apatite layer on the surface of the sample, and the rather flat and homogeneous surface of the cement became more porous and inhomogeneous.

CONCLUSIONS

Addition of synthesized nano-fluoroapatite to as-prepared glass ionomer cement enhanced the compressive strength as well as nucleation of the calcium phosphate layer on the surface of the composite. This makes it a good candidate for dentistry and orthopedic applications.

摘要

问题陈述

为了提高玻璃离子水门汀的性能,人们用金属粉末、短纤维、生物陶瓷等材料对其进行增强。氟磷灰石(Ca(PO)F)存在于牙釉质中,因其良好的化学和物理性质,常用于牙科材料。

目的

本研究考察了添加合成氟磷灰石纳米陶瓷对玻璃离子水门汀抗压强度和生物活性的影响。

材料与方法

将合成的氟磷灰石纳米陶瓷颗粒(约70纳米)掺入制备好的玻璃离子粉末中,并用X射线衍射(XRD)、傅里叶变换红外光谱(FTIR)和扫描电子显微镜(SEM)对其进行表征。此外,还评估了添加0、1、3和5 wt%氟磷灰石的改性玻璃离子水门汀的抗压强度值。

结果

结果表明,与其他组(包括对照组)相比,含有3 wt%氟磷灰石纳米颗粒的玻璃离子水门汀表现出最高的抗压强度(102.6±4)。此外,FTIR和SEM研究表明,将含3 wt%氟磷灰石的玻璃离子水门汀复合材料浸泡在模拟体液溶液中后,由于样品表面形成了磷灰石层,O-H、P-O和C-O吸收带的强度增加,并且水门汀原本相当平坦和均匀的表面变得更加多孔和不均匀。

结论

向制备好的玻璃离子水门汀中添加合成纳米氟磷灰石可提高抗压强度以及复合材料表面磷酸钙层的成核作用。这使其成为牙科和骨科应用的良好候选材料。

https://cdn.ncbi.nlm.nih.gov/pmc/blobs/7fb5/5608063/692d2acfa715/JDB-3-276-g001.jpg

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