Sm Mousavinasab, M Atai, N Salehi, A Salehi
Dental Materials Research Center and Department of Operative Dentistry, School of Dentistry, Isfahan University of Medical Sciences, Isfahan, Iran.
Department of Polymer Science, Iran Polymer and Petrochemical Institute, Tehran, Iran.
J Dent Biomater. 2016 Dec;3(4):299-305.
The degree of conversion depends on the material composition, light source properties, distance from light source, light intensity, curing time, and other factors such as shade and translucency.
In the present study, we evaluated the effects of different light-curing modes and shades of methacrylate and silorane-based resin composites on the degree of conversion of resin composites (DC).
The methacrylate-based (Filtek Z250, 3M, ESPE) and low-shrinkage silorane-based (Filtek P90, 3M, ESPE) resin composites were used in three groups as follows: group 1-Filtek Z250 (shade A3), group 2-Filtek Z250 (shade B2), and group 3-Filtek P90 (shade A3). We used a light-emitting diode (LED) curing unit for photopolymerization. 10 samples were prepared in each group to evaluate the degree of conversion; 5 samples were cured using soft-start curing mode, and the other 5 were cured using standard curing mode. The DC of the resin composites was measured using Fourier Transform Infrared Spectroscopy (FTIR). The data were analyzed using Kruskal Wallis and one-way ANOVA statistical tests.
The degree of conversion of silorane-based resin composite was 70 - 75.8% and that of methacrylate-based resin composites was 60.2 - 68.2% (p = 0.009). The degree of conversion of the composite with brighter colour (B2) was statistically more than the darker composite (A3). Higher degree of conversion was achieved applying the standard curing mode.
The results of the study showed that the colour and type of the resin composite and also the curing mode influence the degree of conversion of resin composites.
转化率取决于材料成分、光源特性、与光源的距离、光强度、固化时间以及其他因素,如色泽和透明度。
在本研究中,我们评估了不同光固化模式以及甲基丙烯酸酯类和硅氧烷类树脂复合材料的色泽对树脂复合材料转化率(DC)的影响。
甲基丙烯酸酯类(Filtek Z250,3M,ESPE)和低收缩硅氧烷类(Filtek P90,3M,ESPE)树脂复合材料分为以下三组使用:第1组 - Filtek Z250(色泽A3),第2组 - Filtek Z250(色泽B2),第3组 - Filtek P90(色泽A3)。我们使用发光二极管(LED)固化单元进行光聚合。每组制备10个样品以评估转化率;5个样品采用软启动固化模式固化,另外5个采用标准固化模式固化。使用傅里叶变换红外光谱(FTIR)测量树脂复合材料的DC。数据采用Kruskal Wallis和单因素方差分析统计检验进行分析。
硅氧烷类树脂复合材料的转化率为70 - 75.8%,甲基丙烯酸酯类树脂复合材料的转化率为60.2 - 68.2%(p = 0.009)。色泽较亮(B2)的复合材料的转化率在统计学上高于色泽较深的复合材料(A3)。采用标准固化模式可实现更高的转化率。
研究结果表明,树脂复合材料的色泽和类型以及固化模式会影响树脂复合材料的转化率。