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自粘接可流动树脂复合材料树脂-牙本质界面的界面显微镜检查及化学分析

Interfacial microscopic examination and chemical analysis of resin-dentin interface of self-adhering flowable resin composite.

作者信息

Hamdy Tamer M

机构信息

Restorative and Dental Materials Department, National Research Centre (NRC), El Bohouth St., 12622 Dokki, Giza, Egypt.

Dr. Tamer Hamdy Dental Clinic, Giza, Egypt.

出版信息

F1000Res. 2017 Sep 14;6:1688. doi: 10.12688/f1000research.12306.4. eCollection 2017.

Abstract

The newly introduced self-adhering flowable resin-composites decrease the required time for application by incorporation of an acidic adhesive monomer, thus reducing the number of steps, but its bonding is still uncertain. The aim of this study was to evaluate the interfacial microscopic examination and chemical analysis at the resin-dentin interface of a self-adhering flowable resin composite (Vertise™Flow Self-Adhering Flowable Composite, Kerr Dental, USA) versus a total-etch (Te-Econom Plus) resin composite, using an etching agent (Eco-Etch gel) and bonding agent (Single Bond Universal). Sixteen freshly extracted sound human posterior teeth were used. The teeth were randomly divided into two groups: 8 specimens per type of composite. Standard-shaped class V cavities were prepared on the buccal surface. One group was restored by Te-Econom Plus resin composite by total-etch technique using Eco-Etch gel, which was applied to dentine for 15 seconds, followed by rinsing, drying and bonding agent application (Single Bond Universal). The other group restored directly with self-adhering resin composite (Vertise-Flow) without application of etch or bond. Curing was done for 20 seconds using a light emitting diode light curing unit. Evaluation of the resin-dentin interface was done microscopically by examination of marginal gap distance in μm using scanning electron microscope (SEM), and chemical analysis of silver particles was observed using SEM with energy-dispersive X-ray spectrometry after 24 hours of specimen storage in ammoniacal silver nitrate. Regarding marginal gap distance (µm) and silver atomic % mean values, teeth restored with self-adhering resin composite (Vertise-Flow) showed significantly higher mean values than the multi-step etch and rinse resin composite group (5.2 0; 12.2 8.2, respectively). Resin-dentin bonding using total-etch resin composite technique was more effective than self-adhering flowable resin composite (Vertise-Flow) regarding marginal gap formation and penetration of silver particles. Further studies for bond strength could be performed.

摘要

新推出的自粘结可流动树脂复合材料通过加入酸性粘结单体减少了应用所需时间,从而减少了步骤数量,但其粘结效果仍不确定。本研究的目的是使用蚀刻剂(Eco-Etch凝胶)和粘结剂(Single Bond Universal),评估一种自粘结可流动树脂复合材料(Vertise™Flow自粘结可流动复合材料,美国科尔牙科公司)与全蚀刻(Te-Econom Plus)树脂复合材料在树脂-牙本质界面的微观检查和化学分析。使用了16颗新拔除的健康人后牙。将牙齿随机分为两组:每种复合材料8个样本。在颊面制备标准形状的V类洞。一组通过使用Eco-Etch凝胶的全蚀刻技术用Te-Econom Plus树脂复合材料修复,将其应用于牙本质15秒,然后冲洗、干燥并应用粘结剂(Single Bond Universal)。另一组直接用自粘结树脂复合材料(Vertise-Flow)修复,不进行蚀刻或粘结。使用发光二极管光固化装置固化20秒。通过使用扫描电子显微镜(SEM)检查以微米为单位的边缘间隙距离,对树脂-牙本质界面进行微观评估,并在将样本在硝酸银氨溶液中储存24小时后,使用带有能量色散X射线光谱仪的SEM观察银颗粒的化学分析。关于边缘间隙距离(微米)和银原子百分比平均值,用自粘结树脂复合材料(Vertise-Flow)修复的牙齿显示出的平均值显著高于多步蚀刻和冲洗树脂复合材料组(分别为5.2±0;12.2±8.2)。在边缘间隙形成和银颗粒渗透方面,使用全蚀刻树脂复合材料技术的树脂-牙本质粘结比自粘结可流动树脂复合材料(Vertise-Flow)更有效。可以进行进一步的粘结强度研究。

https://cdn.ncbi.nlm.nih.gov/pmc/blobs/d266/6206611/30c73f5c028c/f1000research-6-18305-g0000.jpg

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