Abdelraouf Rasha M, Mohammed Manar, Abdelgawad Fatma
Biomaterials Department, Faculty of Dentistry, Cairo University, Cairo, Egypt.
Department of Pediatric and Community Dentistry, Faculty of Oral and Dental Medicine, October 6 University, Cairo, Egypt.
Open Access Maced J Med Sci. 2019 Jul 10;7(13):2162-2166. doi: 10.3889/oamjms.2019.579. eCollection 2019 Jul 15.
This study aimed to assess the shear bond strength of a self-adhering flowable resin composite versus a total-etch one to different surfaces of permanent-molars.
Thirty-six sound human permanent molars were used. The teeth were embedded in acrylic blocks, such that their buccal surfaces were shown. The teeth were divided into three groups: Group I: Uncut-Enamel, Group II: Cut-enamel-surfaces with minimal-grinding and Group III: dentin-surfaces. Half of the teeth in each group were used for bonding to a self-adhering flowable resin-composite (Dyad-flow, Kerr, USA). While the other half of each group was bonded to a total-etch flowable resin-composite (Filtek™Z350-XT,3M-ESPE, USA) which necessitate etching and bonding. Teflon-mold was used for constructing resin composite cylinders (3 × 3 mm) over the buccal surfaces. The Dyad-flow was applied in the central hole of the mould placed upon tooth-surface, and then light-cured for 20 seconds. The Filtek-Z350-XT was applied similarly after etching and bonding steps. The teeth were stored in 37°C distilled water for 24 hours. The strength was measured using a universal testing machine and statistically analysed. Modes of failure were studied using digital-microscope.
Mean values of shear bond strength for the Dyad and Filtek-Z350-XT in the uncut-enamel were 3.5 and 24.6MPa respectively, while that for cut-enamel were 4.5 and 12.7MPa respectively (Both highly statistically significant P ≤ 0.01) and in dentin were 4.3 and 6.7MPa respectively (Statistically significant P ≤ 0.05). The failure mode for Dyad was mainly adhesive (un-cut or cut-enamel 83.3% adhesive and 16.7% mixed, while in dentin 100% adhesive). While the modes of failure for Filtek-Z350-XT in enamel, either cut or un-cut, were 50% cohesive and 50% mixed, whereas in dentin 100% adhesive.
Bonding of self-etch ″Dyad-flow″ flowable resin-composite was lower than the total-etch one in enamel and dentin. Thus further material improvement may be required.
本研究旨在评估自粘结可流动树脂复合材料与全酸蚀可流动树脂复合材料在恒牙不同表面的剪切粘结强度。
使用三十六颗健康的人类恒牙。将牙齿嵌入丙烯酸块中,使其颊面暴露。牙齿分为三组:第一组:未切割釉质组;第二组:轻度打磨的切割釉质表面组;第三组:牙本质表面组。每组中一半的牙齿用于粘结自粘结可流动树脂复合材料(Dyad-flow,美国科尔公司)。而每组的另一半则粘结至需要酸蚀和粘结的全酸蚀可流动树脂复合材料(Filtek™Z350-XT,美国3M-ESPE公司)。使用聚四氟乙烯模具在颊面上构建树脂复合材料圆柱体(3×3毫米)。将Dyad-flow应用于放置在牙齿表面的模具中心孔中,然后光固化20秒。在进行酸蚀和粘结步骤后,以类似方式应用Filtek-Z350-XT。将牙齿在37°C蒸馏水中储存24小时。使用万能试验机测量强度并进行统计学分析。使用数字显微镜研究失效模式。
Dyad和Filtek-Z350-XT在未切割釉质中的剪切粘结强度平均值分别为3.5和24.6MPa,在切割釉质中分别为4.5和12.7MPa(两者均具有高度统计学意义,P≤0.01),在牙本质中分别为4.3和6.7MPa(统计学意义,P≤0.05)。Dyad的失效模式主要为粘结性(未切割或切割釉质中83.3%为粘结性,16.7%为混合性,而在牙本质中100%为粘结性)。而Filtek-Z350-XT在釉质(无论切割与否)中的失效模式为50%内聚性和50%混合性,而在牙本质中100%为粘结性。
自酸蚀“Dyad-flow”可流动树脂复合材料在釉质和牙本质中的粘结强度低于全酸蚀材料。因此可能需要进一步改进材料。