Department of Biomaterials Science, Institute of Dentistry, University of Turku, Finland; Turku Clinical Biomaterial Center-TCBC, Institute of Dentistry, University of Turku, Turku, Finland.
Department of Biomaterials Science, Institute of Dentistry, University of Turku, Finland.
Dent Mater. 2018 Apr;34(4):598-606. doi: 10.1016/j.dental.2018.01.002. Epub 2018 Jan 20.
The aim was to evaluate the effect of short glass-fiber/filler particles proportion on fracture toughness (FT) and flexural strength (FS) of an experimental flowable fiber-reinforced composite (Exp-SFRC) with two methacrylate resin formulations. In addition, we wanted to investigate how the fracture-behavior of composite restorations affected by FT values of SFRC-substructure.
Exp-SFRC was prepared by mixing 50wt% of dimethacrylate based resin matrix (bisGMA or UDMA based) to 50wt% of various weight fractions of glass-fiber/particulate filler (0:50, 10:40, 20:30, 30:20, 40:10, 50:0wt%, respectively). FT and FS were determined for each experimental material following standards. Specimens (n=8) were dry stored (37°C for 2 days) before they were tested. Four groups of posterior composite crowns (n=6) composed of different Exp-SFRCs as substructure and surface layer of commercial particulate filler composite were fabricated. Crowns were statically loaded until fracture. Failure modes were visually examined. The results were statistically analysed using ANOVA followed by post hoc Tukey's test.
ANOVA revealed that ratio of glass-fiber/particulate filler had significant effect (p<0.05) on tested mechanical properties of the Exp-SFRC with both monomer systems. Exp-SFRC (50wt%) had significantly higher FT (2.6MPam) and FS (175.5MPa) (p<0.05) compared to non-reinforced material (1.3MPam, 123MPa). Failure mode analysis of crown restorations revealed that FT value of the substructure directly influenced the failure mode.
This study shows that short glass-fibers can significantly reinforce flowable composite resin and the FT value of SFRC-substructure has prior importance, as it influences the crack arresting mechanism.
评估不同短玻璃纤维/填料颗粒比例对两种甲基丙烯酸酯树脂配方实验性可流动纤维增强复合材料(Exp-SFRC)断裂韧性(FT)和弯曲强度(FS)的影响。此外,我们还研究了复合材料修复体的断裂行为如何受到 SFRC 底层 FT 值的影响。
通过将 50wt%的二甲基丙烯酸酯基树脂基质(双酚 GMA 或 UDMA 基)与 50wt%的各种重量分数的玻璃纤维/颗粒填料(分别为 0:50、10:40、20:30、30:20、40:10、50:0wt%)混合来制备 Exp-SFRC。按照标准对每种实验材料的 FT 和 FS 进行测定。在测试之前,将试件(n=8)在 37°C 下干燥储存 2 天。由不同的 Exp-SFRC 作为底层和商业颗粒填料复合材料的表层制作 4 组后牙复合牙冠(n=6)。对牙冠进行静态加载直至断裂。通过肉眼检查观察失效模式。使用方差分析(ANOVA)和事后 Tukey 检验对结果进行统计分析。
ANOVA 显示,玻璃纤维/颗粒填料的比例对两种单体系统的 Exp-SFRC 的测试力学性能有显著影响(p<0.05)。与非增强材料(1.3MPam,123MPa)相比,含 50wt%玻璃纤维的 Exp-SFRC 的 FT(2.6MPam)和 FS(175.5MPa)显著更高(p<0.05)。牙冠修复体失效模式分析表明,底层的 FT 值直接影响失效模式。
本研究表明,短玻璃纤维可以显著增强可流动复合树脂,并且 SFRC 底层的 FT 值具有优先重要性,因为它影响裂纹阻止机制。