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可流动短纤维复合材料的纳米力学性能与吸水性:整体修复技术和分层修复技术的影响

The Nanomechanical Performance and Water Uptake of a Flowable Short Fiber Composite: The Influence of Bulk and Layering Restorative Techniques.

作者信息

Tarjányi Tamás, Jakab András Gábor, Sámi Márton, Bali Krisztián, Rárosi Ferenc, Jarábik Maja Laura, Braunitzer Gábor, Palkovics Dániel, Lassila Lippo, Lempel Edina, Fráter Márk, Garoushi Sufyan

机构信息

Department of Medical Physics and Informatics, University of Szeged, 6720 Szeged, Hungary.

SEMILAB Semiconductor Physics Laboratory Co. Ltd., 1117 Budapest, Hungary.

出版信息

Polymers (Basel). 2025 Jun 2;17(11):1553. doi: 10.3390/polym17111553.

Abstract

This study aimed to evaluate the nanomechanical surface properties and water uptake of a flowable short-fiber-reinforced composite (SFRC) using various restorative techniques in order to assess its potential as a standalone restorative material. Nanoindentation and compressive creep testing were employed to characterize material performance. Three resin composites were examined: a flowable SFRC (everX Flow), a bulk-fill particulate filler composite (PFC), and a conventional PFC. Five experimental groups were established based on the restorative technique: layered PFC, layered SFRC, bulk SFRC, bulk PFC, and a bi-structure combining SFRC and PFC. Ninety standardized specimens (n = 18/group) were fabricated. Static and creep nanoindentation tests were conducted to assess surface properties, and water uptake was measured over a 30-day period. Data were analyzed using one-way ANOVA and Bonferroni post hoc tests. Nanoindentation revealed significant differences in hardness, with bulk PFC exhibiting the lowest values ( < 0.001). Creep testing indicated changes in modulus and viscosity following water storage. Notably, bulk SFRC showed the lowest water absorption ( < 0.001). Overall, bulk-applied SFRC demonstrated favorable nanomechanical properties and reduced water uptake, demonstrating its suitability as a standalone restorative material. Further clinical investigations are recommended to validate its long-term performance.

摘要

本研究旨在评估一种可流动的短纤维增强复合材料(SFRC)在采用各种修复技术时的纳米力学表面性能和吸水性,以评估其作为单一修复材料的潜力。采用纳米压痕和压缩蠕变测试来表征材料性能。研究了三种树脂复合材料:一种可流动的SFRC(everX Flow)、一种大体积填充颗粒填料复合材料(PFC)和一种传统PFC。根据修复技术建立了五个实验组:分层PFC、分层SFRC、大体积SFRC、大体积PFC以及一种结合了SFRC和PFC的双结构。制作了90个标准化试件(每组n = 18)。进行了静态和蠕变纳米压痕测试以评估表面性能,并在30天内测量了吸水性。使用单向方差分析和Bonferroni事后检验对数据进行分析。纳米压痕显示硬度存在显著差异,大体积PFC的硬度值最低(< 0.001)。蠕变测试表明储水后模量和粘度发生了变化。值得注意的是,大体积SFRC的吸水率最低(< 0.001)。总体而言,大体积应用的SFRC表现出良好的纳米力学性能和较低的吸水率,表明其适合作为单一修复材料。建议进行进一步的临床研究以验证其长期性能。

https://cdn.ncbi.nlm.nih.gov/pmc/blobs/317c/12158244/3284efb7d9ed/polymers-17-01553-g001.jpg

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