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多元方法在橄榄油感官分析参考物质稳定性控制中的应用——第二部分:应用。

Multivariate approaches for stability control of the olive oil reference materials for sensory analysis - part II: applications.

机构信息

Department of Analytical Chemistry, Faculty of Science, University of Granada, Granada, Spain.

Agricultural and Fishery Research Institute (IFAPA) Consejería de Agricultura, Pesca y Desarrollo Rural, Junta de Andalucía, Sevilla, Spain.

出版信息

J Sci Food Agric. 2018 Aug;98(11):4245-4252. doi: 10.1002/jsfa.8946. Epub 2018 Mar 25.

Abstract

BACKGROUND

The organoleptic quality of virgin olive oil depends on positive and negative sensory attributes. These attributes are related to volatile organic compounds and phenolic compounds that represent the aroma and taste (flavour) of the virgin olive oil. The flavour is the characteristic that can be measured by a taster panel. However, as for any analytical measuring device, the tasters, individually, and the panel, as a whole, should be harmonized and validated and proper olive oil standards are needed.

RESULTS

In the present study, multivariate approaches are put into practice in addition to the rules to build a multivariate control chart from chromatographic volatile fingerprinting and chemometrics. Fingerprinting techniques provide analytical information without identify and quantify the analytes. This methodology is used to monitor the stability of sensory reference materials.

CONCLUSION

The similarity indices have been calculated to build multivariate control chart with two olive oils certified reference materials that have been used as examples to monitor their stabilities. This methodology with chromatographic data could be applied in parallel with the 'panel test' sensory method to reduce the work of sensory analysis. © 2018 Society of Chemical Industry.

摘要

背景

特级初榨橄榄油的感官质量取决于积极和消极的感官属性。这些属性与挥发性有机化合物和酚类化合物有关,它们代表了特级初榨橄榄油的香气和味道(风味)。风味是可以通过品尝小组测量的特征。然而,就像任何分析测量设备一样,品尝者个人和小组作为一个整体,应该协调和验证,并需要适当的橄榄油标准。

结果

在本研究中,除了从色谱挥发性指纹图谱和化学计量学建立多元控制图的规则外,还采用了多元方法。指纹图谱技术提供了分析信息,而无需识别和定量分析物。该方法用于监测感官参考物质的稳定性。

结论

已经计算了相似性指数,以建立具有两个橄榄油认证参考物质的多元控制图,这些参考物质已被用作监测其稳定性的示例。这种具有色谱数据的方法可以与“小组测试”感官方法并行应用,以减少感官分析的工作量。 © 2018 化学工业协会。

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