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辉光放电条件下氮碳共渗的Ti-6Al-7Nb钛合金的性能

Properties of Ti-6Al-7Nb titanium alloy nitrocarburized under glow discharge conditions.

作者信息

Kajzer Anita, Grzeszczuk Ola, Kajzer Wojciech, Nowińska Katarzyna, Kaczmarek Marcin, Tarnowski Michał, Wierzchoń Tadeusz

机构信息

Faculty of Biomedical Engineering, Silesian University of Technology, Zabrze, Poland.

Faculty of Mining and Geology, Silesian University of Technology, Gliwice, Poland.

出版信息

Acta Bioeng Biomech. 2017;19(4):181-188.

Abstract

PURPOSE

The paper presents the results of physicochemical and mechanical properties of the Ti-6Al-7Nb alloy with surface modified by formation of a diffusive nitrocarburized layer deposited in a low-temperature plasma process. The main aim of the study was to evaluate the influence of steam sterilization and exposure to Ringer's solution on the utility properties of the alloy.

METHODS

Based on the study of the microstructure, roughness, wettability, resistance to pitting corrosion, ion infiltration and mechanical properties, the usefulness of the proposed method of surface treatment for clinical application was proven.

RESULTS

Deposition of the nitrocarburized layer increased the surface roughness and surface hardness, but also reduced the contact angle, and corrosion resistance with respect to the polished surfaces. The nitrocarburized layer is a barrier against the infiltration of ions to the solution and sterilization and exposure to Ringer solution have greater effect on the physicochemical properties rather than on the mechanical ones.

CONCLUSION

It was found that sterilization, and exposure to Ringer's solution greatly affect the change of physicochemical properties rather than mechanical properties for both nitrocarburized layers and the Ti-6Al-7Nb alloy of mechanically polished surface.

摘要

目的

本文介绍了通过低温等离子体工艺形成扩散氮碳共渗层对Ti-6Al-7Nb合金进行表面改性后的物理化学和力学性能结果。本研究的主要目的是评估蒸汽灭菌和暴露于林格氏液对该合金使用性能的影响。

方法

通过对微观结构、粗糙度、润湿性、耐点蚀性、离子渗透和力学性能的研究,证明了所提出的表面处理方法在临床应用中的有效性。

结果

氮碳共渗层的沉积增加了表面粗糙度和表面硬度,但也降低了接触角,并且相对于抛光表面,耐腐蚀性降低。氮碳共渗层是防止离子渗入溶液的屏障,灭菌和暴露于林格氏液对物理化学性能的影响大于对力学性能的影响。

结论

研究发现,对于氮碳共渗层和机械抛光表面的Ti-6Al-7Nb合金,灭菌和暴露于林格氏液对物理化学性能变化的影响远大于对力学性能的影响。

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Evaluation of the mechanical properties of powder metallurgy Ti-6Al-7Nb alloy.粉末冶金Ti-6Al-7Nb合金力学性能评估
J Mech Behav Biomed Mater. 2017 Mar;67:110-116. doi: 10.1016/j.jmbbm.2016.12.005. Epub 2016 Dec 9.

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